Effects of volume fraction of short-cut quartz fibers on mechanical and thermal properties of SiO2f/SiO2 composites

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS
Donghai Ding, Wangjiao Ding, Jiexin Jiao, Shaonan Liu, Endong Jin, Guoqing Xiao, Li Zhang, Changkun Lei, Chunzhuo Feng, Yanjun Li
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Abstract

SiO2f/SiO2 composites were prepared by compression molding and sintering using short-cut quartz fibers as reinforcement. The effects of fiber volume fraction (15%∼35%) on bulk density, apparent porosity, and mechanical and thermal properties of the composites were investigated. The results indicated that the samples with 25% fiber volume fraction had the best comprehensive performance, with an apparent porosity and compressive strength of 36% and 46.3 MPa, respectively. The flexural strength of the samples was 13.9 MPa, which represented a 90% increase compared to the samples without fibers. It was attributed to the occurrence of fiber debonding and fiber pull-out in the porous matrix. Meanwhile, the residual strength ratio of the samples after 20 thermal shocks was 74.8%. In addition, the average coefficient of thermal expansion was 0.95 × 10− 6/℃ at 300 ℃∼700 ℃ and the thermal conductivity was 0.388 W·m− 1·K− 1 at 800 °C. This approach can satisfy the requirements of low cost, fast preparation of SiO2f/SiO2 composites, which offers the prospect of its application in the integration of load-bearing and thermal insulation.

Abstract Image

短切石英纤维体积分数对 SiO2f/SiO2 复合材料机械性能和热性能的影响
使用短切石英纤维作为增强材料,通过压缩成型和烧结制备了 SiO2f/SiO2 复合材料。研究了纤维体积分数(15%∼35%)对复合材料的体积密度、表观孔隙率、力学性能和热性能的影响。结果表明,纤维体积分数为 25% 的样品综合性能最好,表观孔隙率和抗压强度分别为 36% 和 46.3 兆帕。样品的抗弯强度为 13.9 兆帕,与不含纤维的样品相比提高了 90%。这归因于多孔基质中纤维的脱粘和纤维的拔出。同时,经过 20 次热冲击后,样品的残余强度比为 74.8%。此外,在 300 ℃∼700 ℃ 时的平均热膨胀系数为 0.95 × 10- 6/℃,在 800 ℃ 时的热导率为 0.388 W-m- 1-K-1。这种方法可以满足低成本、快速制备 SiO2f/SiO2 复合材料的要求,为其在承重和隔热一体化中的应用提供了前景。
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来源期刊
Journal of the Australian Ceramic Society
Journal of the Australian Ceramic Society Materials Science-Materials Chemistry
CiteScore
3.70
自引率
5.30%
发文量
123
期刊介绍: Publishes high quality research and technical papers in all areas of ceramic and related materials Spans the broad and growing fields of ceramic technology, material science and bioceramics Chronicles new advances in ceramic materials, manufacturing processes and applications Journal of the Australian Ceramic Society since 1965 Professional language editing service is available through our affiliates Nature Research Editing Service and American Journal Experts at the author''s cost and does not guarantee that the manuscript will be reviewed or accepted
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