Laser powder bed fusion of WE43 magnesium alloy with superior balance of strength and ductility

IF 15.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING
Wenhe Xu , Jikang Li , Zhenwu Zhang , Hongwei Yuan , Guojin An , Hai Shi , Chao Cai , Wenming Jiang , Wei Li , Qingsong Wei
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Abstract

WE43 is a high-strength magnesium alloy containing rare-earth elements such as Y, Gd and Nd. Nevertheless, how to further obtain the balance of strength and ductility, as well as the manufacture of complex structures is still a dilemma for its engineering application. In this study, WE43 alloy samples with fine microstructures, high densification and excellent mechanical properties were successfully prepared by laser powder bed fusion (LPBF) additive manufacturing. The optimal process window was established, and the formation mechanisms of three types of porosity defects were revealed, namely lack-of-fusion pores, melt fluctuation-induced pores, and keyhole-induced pores. With the combined process of laser power of 200 W and scanning speed of 600 mm/s, samples with a high density of 99.89% were obtained. Furthermore, periodic heterogeneous microstructure was prepared along the build direction, i.e., fine grains (∼4.1 µm) at melt pool boundaries and coarse grain (∼23.6 µm) inside melt pool. This was mainly due to the preferential precipitation of Zr and Mg3(Gd, Nd) nano-precipitates at the melt pool boundaries providing nucleation sites for the grains. This special feature could provide an extra hetero-deformation induced (HDI) strengthening and retard fracture. The optimal tensile yield strength, ultimate tensile strength and elongation at break were 276 ± 1 MPa, 292 ± 1 MPa and 6.1 ± 0.2%, respectively. The obtained tensile properties were superior to those of other magnesium alloys and those fabricated by other processes. The solid solution strengthening (∼24.5%), grain boundary strengthening (∼14.4%) and HDI strengthening (∼32.2%) were the main sources of high yield strength. This work provides a guidance on studying the pore defect suppression and strengthening mechanisms of WE43 alloy and other magnesium alloys produced by LPBF.
激光粉末床熔融 WE43 镁合金,实现强度和延展性的卓越平衡
WE43是一种含Y、Gd、Nd等稀土元素的高强度镁合金。然而,如何进一步获得强度和延性的平衡,以及复杂结构的制造,仍然是其工程应用的难题。本研究采用激光粉末床熔合(LPBF)增材制造技术成功制备了显微组织精细、致密化程度高、力学性能优异的WE43合金样品。建立了最佳工艺窗口,揭示了三种类型气孔缺陷的形成机理,即熔体波动诱导气孔、熔体波动诱导气孔和锁孔诱导气孔。在激光功率为200 W,扫描速度为600 mm/s的组合工艺下,获得了密度高达99.89%的样品。此外,沿着构建方向制备了周期性的非均匀微观结构,即熔池边界处的细晶粒(~ 4.1µm)和熔池内的粗晶粒(~ 23.6µm)。这主要是由于Zr和Mg3(Gd, Nd)纳米相在熔池边界优先析出,为晶粒提供了成核位置。这种特殊的特性可以提供额外的异质变形诱导(HDI)强化和延迟断裂。最佳抗拉屈服强度、极限抗拉强度和断裂伸长率分别为276±1 MPa、292±1 MPa和6.1±0.2%。得到的拉伸性能优于其他镁合金及其他工艺制备的镁合金。固溶强化(~ 24.5%)、晶界强化(~ 14.4%)和HDI强化(~ 32.2%)是高屈服强度的主要来源。该工作对研究LPBF制备的WE43合金及其他镁合金的孔隙缺陷抑制和强化机理具有指导意义。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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