Wenhe Xu , Jikang Li , Zhenwu Zhang , Hongwei Yuan , Guojin An , Hai Shi , Chao Cai , Wenming Jiang , Wei Li , Qingsong Wei
{"title":"Laser powder bed fusion of WE43 magnesium alloy with superior balance of strength and ductility","authors":"Wenhe Xu , Jikang Li , Zhenwu Zhang , Hongwei Yuan , Guojin An , Hai Shi , Chao Cai , Wenming Jiang , Wei Li , Qingsong Wei","doi":"10.1016/j.jma.2024.03.012","DOIUrl":null,"url":null,"abstract":"<div><div>WE43 is a high-strength magnesium alloy containing rare-earth elements such as Y, Gd and Nd. Nevertheless, how to further obtain the balance of strength and ductility, as well as the manufacture of complex structures is still a dilemma for its engineering application. In this study, WE43 alloy samples with fine microstructures, high densification and excellent mechanical properties were successfully prepared by laser powder bed fusion (LPBF) additive manufacturing. The optimal process window was established, and the formation mechanisms of three types of porosity defects were revealed, namely lack-of-fusion pores, melt fluctuation-induced pores, and keyhole-induced pores. With the combined process of laser power of 200 W and scanning speed of 600 mm/s, samples with a high density of 99.89% were obtained. Furthermore, periodic heterogeneous microstructure was prepared along the build direction, i.e., fine grains (∼4.1 µm) at melt pool boundaries and coarse grain (∼23.6 µm) inside melt pool. This was mainly due to the preferential precipitation of Zr and Mg<sub>3</sub>(Gd, Nd) nano-precipitates at the melt pool boundaries providing nucleation sites for the grains. This special feature could provide an extra hetero-deformation induced (HDI) strengthening and retard fracture. The optimal tensile yield strength, ultimate tensile strength and elongation at break were 276 ± 1 MPa, 292 ± 1 MPa and 6.1 ± 0.2%, respectively. The obtained tensile properties were superior to those of other magnesium alloys and those fabricated by other processes. The solid solution strengthening (∼24.5%), grain boundary strengthening (∼14.4%) and HDI strengthening (∼32.2%) were the main sources of high yield strength. This work provides a guidance on studying the pore defect suppression and strengthening mechanisms of WE43 alloy and other magnesium alloys produced by LPBF.</div></div>","PeriodicalId":16214,"journal":{"name":"Journal of Magnesium and Alloys","volume":"13 3","pages":"Pages 1275-1293"},"PeriodicalIF":15.8000,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Magnesium and Alloys","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2213956724001063","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
引用次数: 0
Abstract
WE43 is a high-strength magnesium alloy containing rare-earth elements such as Y, Gd and Nd. Nevertheless, how to further obtain the balance of strength and ductility, as well as the manufacture of complex structures is still a dilemma for its engineering application. In this study, WE43 alloy samples with fine microstructures, high densification and excellent mechanical properties were successfully prepared by laser powder bed fusion (LPBF) additive manufacturing. The optimal process window was established, and the formation mechanisms of three types of porosity defects were revealed, namely lack-of-fusion pores, melt fluctuation-induced pores, and keyhole-induced pores. With the combined process of laser power of 200 W and scanning speed of 600 mm/s, samples with a high density of 99.89% were obtained. Furthermore, periodic heterogeneous microstructure was prepared along the build direction, i.e., fine grains (∼4.1 µm) at melt pool boundaries and coarse grain (∼23.6 µm) inside melt pool. This was mainly due to the preferential precipitation of Zr and Mg3(Gd, Nd) nano-precipitates at the melt pool boundaries providing nucleation sites for the grains. This special feature could provide an extra hetero-deformation induced (HDI) strengthening and retard fracture. The optimal tensile yield strength, ultimate tensile strength and elongation at break were 276 ± 1 MPa, 292 ± 1 MPa and 6.1 ± 0.2%, respectively. The obtained tensile properties were superior to those of other magnesium alloys and those fabricated by other processes. The solid solution strengthening (∼24.5%), grain boundary strengthening (∼14.4%) and HDI strengthening (∼32.2%) were the main sources of high yield strength. This work provides a guidance on studying the pore defect suppression and strengthening mechanisms of WE43 alloy and other magnesium alloys produced by LPBF.
期刊介绍:
The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.