The Effect of Hydrothermal Aging on The Color Stability of Gradient Zirconia. In Vitro Study

Mennat Allah Ramadan, Hanaa Zaghloul, Tamer Hamza
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Abstract

Aim: The study aims to assess the influence of hydrothermal aging on gradient zirconia's microstructure and color stability. Materials and methods: Ten discs were constructed from gradient zirconia blanks (3Y-TZP-5Y-TZP) using CAD\CAM technology. Hydrothermal aging was done in an autoclave. Color parameters (a*, b*, L*) for each disc was measured using a spectrophotometer. In order to investigate the zirconia specimens' crystalline structure, X-ray diffraction (XRD) was performed. Color stability and microstructural changes were examined before and after the aging process. Results: Following hydrothermal aging, a statistically significant decrease in the mean (L*) value was found. However, following hydrothermal aging, a statistically significant increase in the mean (a*) and (b*) values was reported. Regarding the microstructure, hydrothermal aging did not result in any significant changes. Conclusion: Artificial aging has led to color changes in gradient zirconia that were in the clinical acceptability range but has no impact on the microstructure of gradient zirconia.
水热老化对梯度氧化锆颜色稳定性的影响。体外研究
目的:本研究旨在评估水热老化对梯度氧化锆微观结构和颜色稳定性的影响。材料和方法:使用 CAD/CAM 技术,用梯度氧化锆坯料(3Y-TZP-5Y-TZP)制作十个牙盘。在高压釜中进行水热老化。使用分光光度计测量了每个圆盘的颜色参数(a*、b*、L*)。为了研究氧化锆试样的晶体结构,进行了 X 射线衍射 (XRD)。对老化过程前后的颜色稳定性和微观结构变化进行了检测。结果显示水热老化后,平均 (L*) 值出现了统计学意义上的显著下降。然而,在水热老化后,平均 (a*) 和 (b*) 值在统计上有显著增加。在微观结构方面,水热老化没有导致任何明显变化。结论人工老化导致梯度氧化锆的颜色发生变化,这种变化在临床可接受范围内,但对梯度氧化锆的微观结构没有影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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