Microwave and ultrasound assisted extraction techniques with citric acid of pectin from Pomelo (Citrus maxima) peel

Md. Murad Hossain, Rowshon Ara, Farzana Yasmin, Mahjabin Suchi, Wahidu Zzaman
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Abstract

This current research attempted to obtain pectin from Pomelo (Citrus maxima) peels using conventional heating, microwave-assisted extraction (MAE), and ultrasound-assisted extraction (UAE) techniques with organic citric acid. In order to characterize pectin extracted using conventional heating, MAE, and UAE, yield, pH, solubility, ash content, equivalent weight, anhydrouronic acid content, degree of esterification methoxyl content were taken into consideration. On physicochemical properties, the extraction techniques had a significant effect. The findings demonstrated that the MAE method produced the highest amount of pectin (26.63 ± 0.21 %). On the basis of the Degree of Esterification (DE) value, pectins were all classified as high-methoxypectins (HMP). According to anhydrouronic acid (AUA) content, the extracted pectins were extremely pure. Fourier transform infrared (FT-IR) spectroscopy was used to structurally characterize pectin that was extracted using three different methods, and the results revealed that pectin has functional groups between 1740 and 800 cm-1 spectrally.

微波和超声波辅助柠檬酸提取柚子(Citrus maxima)果皮中果胶的技术
本研究试图利用传统加热、微波辅助萃取(MAE)和超声辅助萃取(UAE)技术从柚子(Citrus maxima)果皮中提取果胶,并加入有机柠檬酸。为了确定采用传统加热、微波辅助萃取和超声辅助萃取技术提取的果胶的特性,研究人员考虑了产量、pH 值、溶解度、灰分含量、当量重量、无水酸含量、酯化程度、甲氧基含量等因素。萃取技术对理化性质有显著影响。研究结果表明,MAE 法提取的果胶含量最高(26.63 ± 0.21 %)。根据酯化度(DE)值,果胶均被归类为高甲氧基pectins(HMP)。根据无水酸(AUA)含量,提取的果胶纯度极高。傅立叶变换红外光谱(FT-IR)用于分析用三种不同方法提取的果胶的结构特征,结果表明果胶在光谱上具有 1740 至 800 cm-1 之间的官能团。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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CiteScore
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