Preparation of nitrogen-doped carbon materials by orthogonal array design for supercapacitors

IF 1.5 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY
Cungui Zhong, Dayong Liu
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引用次数: 0

Abstract

Here, the authors report a practical method for preparing nitrogen-doped carbon materials using an orthogonal array design. The material with the highest specific capacitance value of 262 F·g−1 at a current density of 1 A·g−1 was obtained under the conditions (KOH as activation agent, activation temperature of 600°C, activation time of 3 h, respectively). Its high electrochemical properties are attributed to its high surface area and additional pseudo-capacitance. After 5000 cycles, the specific capacitance remained 92.8%, with good cycle stability. Textural characterization of the carbon materials was performed using N2 adsorption/desorption and scanning electron microscopy.

Abstract Image

通过正交阵列设计制备用于超级电容器的掺氮碳材料
在此,作者报告了一种利用正交阵列设计制备掺氮碳材料的实用方法。在此条件下(分别以 KOH 作为活化剂、活化温度为 600°C、活化时间为 3 小时),获得了电流密度为 1 A-g-1 时比电容值最高的 262 F-g-1 材料。其较高的电化学特性归功于其较高的表面积和额外的假电容。经过 5000 次循环后,比电容保持在 92.8%,具有良好的循环稳定性。利用 N2 吸附/解吸和扫描电子显微镜对碳材料进行了纹理表征。
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来源期刊
Micro & Nano Letters
Micro & Nano Letters 工程技术-材料科学:综合
CiteScore
3.30
自引率
0.00%
发文量
58
审稿时长
2.8 months
期刊介绍: Micro & Nano Letters offers express online publication of short research papers containing the latest advances in miniature and ultraminiature structures and systems. With an average of six weeks to decision, and publication online in advance of each issue, Micro & Nano Letters offers a rapid route for the international dissemination of high quality research findings from both the micro and nano communities. Scope Micro & Nano Letters offers express online publication of short research papers containing the latest advances in micro and nano-scale science, engineering and technology, with at least one dimension ranging from micrometers to nanometers. Micro & Nano Letters offers readers high-quality original research from both the micro and nano communities, and the materials and devices communities. Bridging this gap between materials science and micro and nano-scale devices, Micro & Nano Letters addresses issues in the disciplines of engineering, physical, chemical, and biological science. It places particular emphasis on cross-disciplinary activities and applications. Typical topics include: Micro and nanostructures for the device communities MEMS and NEMS Modelling, simulation and realisation of micro and nanoscale structures, devices and systems, with comparisons to experimental data Synthesis and processing Micro and nano-photonics Molecular machines, circuits and self-assembly Organic and inorganic micro and nanostructures Micro and nano-fluidics
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