{"title":"Preparation of nitrogen-doped carbon materials by orthogonal array design for supercapacitors","authors":"Cungui Zhong, Dayong Liu","doi":"10.1049/mna2.12189","DOIUrl":null,"url":null,"abstract":"<p>Here, the authors report a practical method for preparing nitrogen-doped carbon materials using an orthogonal array design. The material with the highest specific capacitance value of 262 F·g<sup>−1</sup> at a current density of 1 A·g<sup>−1</sup> was obtained under the conditions (KOH as activation agent, activation temperature of 600°C, activation time of 3 h, respectively). Its high electrochemical properties are attributed to its high surface area and additional pseudo-capacitance. After 5000 cycles, the specific capacitance remained 92.8%, with good cycle stability. Textural characterization of the carbon materials was performed using N<sub>2</sub> adsorption/desorption and scanning electron microscopy.</p>","PeriodicalId":18398,"journal":{"name":"Micro & Nano Letters","volume":"19 1","pages":""},"PeriodicalIF":1.5000,"publicationDate":"2024-01-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1049/mna2.12189","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Micro & Nano Letters","FirstCategoryId":"88","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1049/mna2.12189","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
Here, the authors report a practical method for preparing nitrogen-doped carbon materials using an orthogonal array design. The material with the highest specific capacitance value of 262 F·g−1 at a current density of 1 A·g−1 was obtained under the conditions (KOH as activation agent, activation temperature of 600°C, activation time of 3 h, respectively). Its high electrochemical properties are attributed to its high surface area and additional pseudo-capacitance. After 5000 cycles, the specific capacitance remained 92.8%, with good cycle stability. Textural characterization of the carbon materials was performed using N2 adsorption/desorption and scanning electron microscopy.
期刊介绍:
Micro & Nano Letters offers express online publication of short research papers containing the latest advances in miniature and ultraminiature structures and systems. With an average of six weeks to decision, and publication online in advance of each issue, Micro & Nano Letters offers a rapid route for the international dissemination of high quality research findings from both the micro and nano communities.
Scope
Micro & Nano Letters offers express online publication of short research papers containing the latest advances in micro and nano-scale science, engineering and technology, with at least one dimension ranging from micrometers to nanometers. Micro & Nano Letters offers readers high-quality original research from both the micro and nano communities, and the materials and devices communities.
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