Green synthesis of Nickel Oxide Nanoparticles using Syzygium Aromatic Extract: Characterization and Biological Applications

Shaimaa M. Jassim, Mohammed A. Abd, Israa A. Hammed
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Abstract

In this study, nickel oxide (NiO) nanoparticles were successfully synthesized by Syzygium aromaticum (clove) extract via a green synthesis method and evaluated their antibacterial properties. The bio-molecules inside the extract play an important role in converting nickel nitrate salt into nickel oxide nanoparticles. The prepared nickel oxide nanoparticles were characterized via different techniques such as X-ray Diffraction, fourier transform infrared spectroscopy, field emission-scanning electron microscopy and ultraviolet-visible spectrophotometer. From X-ray diffraction results, the crystallite size of NiO NPs was estimated to be (39.7 nm). The fourier transform infrared spectroscopy exhibits intense two peaks at 594 cm-1 and 469 cm-1 which indicates the formation of NiO NPs. In addition, the energy band-gap calculated by Tauc’s formula was ~ 2.89 eV. Finally, The antibacterial activity study results detected that NiO NPs have the highest activity against Staphylococcus aureus when compared to Escherichia coli. Thus, the present study exhibits good antibacterial activity, which may be explored in future clinical treatments.
绿色合成氧化镍纳米粒子的紫丁香芳香提取物:表征和生物应用
本研究以丁香提取物为原料,采用绿色合成方法成功合成了氧化镍纳米颗粒,并对其抗菌性能进行了评价。萃取物中的生物分子在硝酸镍转化为氧化镍纳米颗粒的过程中起着重要作用。采用x射线衍射、傅里叶变换红外光谱、场发射扫描电镜和紫外可见分光光度计等技术对制备的氧化镍纳米颗粒进行了表征。根据x射线衍射结果,估计NiO NPs的晶粒尺寸为(39.7 nm)。傅里叶变换红外光谱在594 cm-1和469 cm-1处有两个强烈的峰,表明NiO NPs的形成。此外,由Tauc公式计算的能带隙为~ 2.89 eV。最后,抑菌活性研究结果发现,NiO NPs对金黄色葡萄球菌的抑菌活性高于大肠杆菌。因此,本研究显示出良好的抗菌活性,可以在未来的临床治疗中进行探索。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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