OPTIMASI RASIO Si/Al, RASIO PADATAN/CAIRAN, KONSENTRASI NaOH DAN JENIS AGREGAT DALAM SINTESA BETON GEOPOLIMER DENGAN METODE TAGUCHI

Ufafa Anggarini
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Abstract

The optimization synthezised of geopolymer based on fly ash materials have been done by using Taguchi method. The experimental design was done with 4 factors and 3 levels, that were the influence of Si/Al ratio, solid/liquid ratio, NaOH and the type of aggregate. Geopolymers were synthesized by sol gel method at room temperature, using fly ash as aluminasilica source and alkaline activator solutions thain consist of NaOH and Na2SiO3. The influence of Si/Al ratio studied at level of 4.00, 4.25, 4,50, solid/liquid ratio at level of 1.50, 2.33, 4.00. NaOH (%wt/%v) of 0.24, 0.40, 0.56, and the type of aggregate of Malang sand, Bojonegoro sand and granite. Based on SNR analysis and the characterization determination of higher is better, the geopolymer optimum composition was Si/Al factor at level of 3 (4.50), solid/liquid ratio level at 2 (2.33), NaOH level at 1 (0.24) and type of aggregate level at 3 (granite). The calculation of compressive strength prediction was determined at 21.01 Mpa, while the optimum compressive strength of the experimental result was found at 21 Mpa. Keywords: Geopolymer, Taguchi Method, Si/Al, Solid/Liquid, NaOH, Type of agreggate
优化Si/Al比,固体/液体比
采用田口法对粉煤灰基地聚合物进行了优化合成。采用硅铝比、料液比、氢氧化钠和骨料类型4因素3水平进行试验设计。以粉煤灰为硅铝源,以NaOH和Na2SiO3为碱性活化剂,在室温下采用溶胶-凝胶法制备地聚合物。研究了硅铝比在4.00、4.25、4、50水平和固液比在1.50、2.33、4.00水平下的影响。NaOH (%wt/%v)分别为0.24、0.40、0.56,与麻郎砂、波戎内戈罗砂和花岗岩的骨料类型有关。基于信噪比分析和越高越好的表征判定,地聚合物的最佳组成为Si/Al因子水平为3(4.50),料液比水平为2 (2.33),NaOH水平为1(0.24),骨料类型水平为3(花岗岩)。在21.01 Mpa时确定了抗压强度预测计算值,在21 Mpa时确定了试验结果的最佳抗压强度。关键词:地聚合物,田口法,硅/铝,固/液,氢氧化钠,骨料类型
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