Obtaining of aluminum nano-powders by thermal treatment

G. Paskalov, Usa Plasma Microsystems Llc
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Abstract

It is known that the formation of a dispersed phase under extreme conditions (high temperatures andprocess speed) leads to the formation of a non-equilibrium structure of particles. Therefore, the first toattract attention are technologies based on pulsed processes with high rates of change in the thermodynamicparameters of the system. One of these promising methods for obtaining a wide range of nano-powders ofinorganic materials is the technology based on the process of electrical explosion of a conductor (EVP, EVPtechnology) [1-5]. Unfortunately, this method is not applicable on industrial scales. In this thesis, productionof Al nanoparticles by hydrogen reduction of metal chlorides in gas phase was studied. Nanoparticles haveunique properties not found in bulk or micron-scale materials. These enable new products or reduced useof raw materials. Metal nanoparticle production has been studied widely, but especially for coated metalparticles, research of coating mechanisms and economic production methods is still needed. The usedmethod combines a high yield, a high production rate, low production costs, high particle quality, and agood range of available particle number average diameters and other properties. Control of the productparameters has been carried out by using a special quenching system and plasma reactor configuration.Highly hydrogen enriched Al nanopowder were collected in metal form and tested for different applications.
热处理法制备纳米铝粉
众所周知,在极端条件下(高温和加工速度),分散相的形成会导致颗粒的非平衡结构的形成。因此,首先引起注意的是基于系统热力学参数高变化率的脉冲过程的技术。基于导体电爆炸过程的技术(EVP, EVP技术)是获得多种无机材料纳米粉末的有前途的方法之一[1-5]。不幸的是,这种方法不适用于工业规模。本文研究了气相氢还原金属氯化物制备纳米铝的方法。纳米颗粒具有在块状或微米级材料中所没有的独特性质。这使得新产品或减少原材料的使用成为可能。金属纳米颗粒的制备已经得到了广泛的研究,但对于包覆金属颗粒,还需要对包覆机理和经济生产方法进行研究。该方法具有产率高、生产率高、生产成本低、颗粒质量高、可用颗粒数、平均直径范围广等特点。通过使用特殊的淬火系统和等离子体反应器配置对产品参数进行了控制。以金属形式收集了高富氢铝纳米粉,并对其进行了不同用途的测试。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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