In situ analysis utilizing electrical resistance measurements when brazing cemented carbides

W. Tillmann, N. Sievers, A. Schmidt, C. Timmer
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Abstract

Abstract Usually it is not possible to observe a high temperature brazing process such as joining cemented carbides to steel with copper as filler metal. The process takes place in a vacuum chamber at high temperatures and an analysis of the joint formed is only possible in a subsequent step. In this investigation, a novel setup has been introduced to allow for an in situ measurement of the brazing process via its electrical resistance. For this, a 4wiretechnique has been applied to the specimen to precisely measure the low resistance of the joint within a range of µΩ. By choosing two different holding times at a process temperature of 1150 °C and by analyzing the ensuing joint structures, it was possible to correlate the signal measured with the on-going diffusion and bonding process. Finally, the authors have revealed that the applied current of the measurement system had a distinct effect on the joint structure formed, which could be used additionally to improve the quality of the joint.
在钎焊硬质合金时利用电阻测量进行现场分析
摘要通常不可能观察到以铜作为填充金属将硬质合金与钢连接的高温钎焊过程。该过程在高温的真空室中进行,只有在后续步骤中才能对形成的接头进行分析。在本研究中,引入了一种新的设置,允许通过其电阻对钎焊过程进行现场测量。为此,在试样上应用了4wire技术,以在µΩ范围内精确测量关节的低电阻。通过在1150°C的工艺温度下选择两种不同的保温时间,并通过分析随后的接头结构,可以将测量到的信号与正在进行的扩散和键合过程相关联。最后,作者揭示了测量系统施加的电流对形成的接头结构有明显的影响,可以用来提高接头的质量。
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