Acid Etch Study of Vertically Aligned Carbon Nanofibers (VACNFs)

Zhuxin Dong, U. Wejinya, S. N. S. Chalamalasetty, M. R. Margis, T. G. Duensing
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Abstract

One of the major limitations in the development of ultrasensitive electrochemical biosensors based on one dimensional nanostructures is the difficulty involved with uniform growth of the nanofibers. Fabrication of the Vertically Aligned Carbon Nano Fibers (VACNFs) involve treatment of several chemicals including a variety of etchants. In previous work, successful measurement and characterization of electron beam patterned VACNFs is demonstrated using Atomic Force Microscopy. Also the effect of most commonly used etchant i.e. HF is studied. Here, the effect of acid etching on VACNFs is observed and characterized using a highly sensitive and precise Atomic Force Microscopy (AFM). Furthermore, statistical analysis is performed on AFM data to demonstrate data confidence and verify experiments.
垂直排列纳米碳纤维(VACNFs)的酸蚀研究
基于一维纳米结构的超灵敏电化学生物传感器发展的主要限制之一是纳米纤维难以均匀生长。垂直排列碳纳米纤维(VACNFs)的制备涉及多种化学品的处理,包括各种蚀刻剂。在以前的工作中,利用原子力显微镜成功地测量和表征了电子束图像化的vacnf。同时还研究了最常用的蚀刻剂HF的影响。在这里,使用高灵敏度和精确的原子力显微镜(AFM)观察和表征酸蚀刻对vacnf的影响。此外,对AFM数据进行了统计分析,以证明数据的置信度和验证实验。
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