CHARACTERIZATION OF 3D-PRINTING FILAMENT WITH EXTRUDER MELTING TEMPERATURE VARIATION FOR BONE IMPLANT FROM KUPANG SHELL

Ananda Maulidha Kusumastuti, Adik Roni Setiawan, Asalina Putri Agung Shaliha, Deden Eko Wiyono, Achmad Ferdiansyah Pradana Putra
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Abstract

The number of bone damage in Indonesia continues to increase. Bone implant is one of the medical treatment methods performed on bone damage. Organic and non-organic materials can be used as bone implants. Non-organic materials are stronger, but not biocompatible, while organic materials are biocompatible, but brittle. The addition of polycaprolactone polymer (PCL) can increase the mechanical strength of 3D printing bone implant filaments. Extruder melting temperature is one of the factors that affect the quality of PCL-HAp filaments for bone implants. Studies related to temperature variations in PCL-HAp materials have not been widely studied. Therefore, it is necessary to characterize 3D printing filaments with variations in the melting temperature of the extruder as bone implants from mussel shells with temperature variables of 65oC, 75oC, and 85oC. From this study, the optimum point was found at the melting extruder temperature of 75oC with the results of a diameter of 1.810 and mechanical strength which showed an increase in tensile strength and Young's modulus of PCL-HAp composite in all variables compared to pure PCL. The SEM test showed a rough surface on the filaments that could increase the proliferation and adhesion of good cells for the growth of bone tissue.
利用挤出机熔融温度变化3d打印古邦壳骨植入材料的研究
在印度尼西亚,骨损伤的数量持续增加。骨植入是骨损伤的医学治疗方法之一。有机和非有机材料都可以用作骨植入物。非有机材料更强,但不具有生物相容性,而有机材料具有生物相容性,但易碎。聚己内酯聚合物(PCL)的加入可以提高3D打印骨种植体长丝的机械强度。挤出机熔融温度是影响植骨用聚乳酸-羟基磷灰石长丝质量的因素之一。有关PCL-HAp材料温度变化的研究还没有得到广泛的研究。因此,有必要将挤出机熔融温度变化的3D打印细丝表征为贻贝壳骨植入物,温度变量为65℃,75℃和85℃。本研究发现,熔融挤出温度为75℃时的最佳点为直径为1.810,机械强度为1.810,与纯PCL相比,PCL- hap复合材料的抗拉强度和杨氏模量在所有变量中均有所提高。扫描电镜显示,纤维表面粗糙,有利于骨组织生长的良好细胞的增殖和粘附。
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