Synthesis, Characterization and Acetone Sensing Performance of ZnFe2O4 Hollow Spheres/RGO Composites

Kaidi Wu, Yifan Luo, Chao Zhang
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Abstract

ZnFe 2 O 4 hollow spheres and ZnFe 2 O 4 hollow spheres / RGO composites with different RGO contents were successfully synthesized using a one-pot solvothermal method. The morphology and microstructure of the as-prepared samples were characterized through multiple techniques. The gas-sensing experiments include the effects of operating temperature and RGO mixing mass on the gas-sensing response, the selectivity and the response of the sensor based on 0.5 wt% ZnFe 2 O 4 /RGO to acetone in various concentrations. The experimental results reveal that the mixing of graphene into ZnFe 2 O 4 hollow spheres can improve the performance of the sensors to low-ppm-level acetone vapor, and the sensor based on 0.5 wt% ZnFe 2 O 4 /RGO exhibits good sensitivity and selectivity to 0.8-10 ppm acetone vapor at 200℃. So, the sensor based on 0.5 wt% ZnFe 2 O 4 /RGO may be applied to detect diabetes mellitus via quantitative measuring of the acetone from respiratory gases of patients if the response is improved further and the operating temperature is further optimized.
ZnFe2O4空心球/还原氧化石墨烯复合材料的合成、表征及丙酮传感性能
采用一锅溶剂热法制备了不同RGO含量的znfe2o4空心球和znfe2o4空心球/ RGO复合材料。通过多种技术对制备样品的形貌和微观结构进行了表征。气敏实验包括操作温度和RGO混合质量对气敏响应的影响,以及基于0.5 wt% znfe2o /RGO的传感器对不同浓度丙酮的选择性和响应。实验结果表明,将石墨烯掺入znfe2o4空心球中可以提高传感器对低浓度丙酮蒸汽的灵敏度,0.5 wt% znfe2o4 /RGO的传感器对200℃下0.8 ~ 10 ppm丙酮蒸汽具有良好的灵敏度和选择性。因此,如果进一步提高灵敏度和优化工作温度,基于0.5 wt% znfe2o4 /RGO的传感器可以通过定量测量患者呼吸气体中的丙酮来检测糖尿病。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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