optimization Possibilities of properties of niti alloys used as traumatology implants

M. Kopelent, M. Losertová, M. Štencek, K. Konečná, B. Smetana, J. Drápala
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Abstract

Shape memory alloy represents metallic material that can return to its original forms, shapes, or sizes when subjected to a process of memorization between two transformation phases. The basic application of these materials is always simple, i.e. where the material can be easily deformed by an external force and will recover its original forms when heated at a certain temperature. NiTi alloy is mainly characterized by its special properties, namely the shape memory effect and superelastic behavior, as well as the excellent corrosion resistance, high strength, low modulus of elasticity and biocompatibility. Due to its superelasticity, NiTi resembles to some human rigid tissues, including bones and tendons that enables its using in implants or tools for many medical cases in orthopedics, neurology, cardiology, interventional radiology, endodontics, etc. In this work, the effect of thermal treatment on physical-metallurgical properties of NiTi alloy was studied. Flat samples of NiTi alloy with a composition of 50.6 at% Ni and 49.4 at% Ti were solution treated at 850 °C and subsequently aged at 450 °C. The microstructures in as-received, solution treated or solution treated and aged stages were examined by means of optical or scanning electron microscopies. The analysis of the heat treatment effect on the microstructure and transformation temperatures was completed by Vickers microhardness measurement and by differential scanning calorimetry.
镍钛合金创伤植入材料性能的优化
形状记忆合金是一种金属材料,经过两个变形阶段之间的记忆过程,可以恢复到原来的形状、形状或尺寸。这些材料的基本应用总是很简单,即材料在外力作用下容易变形,在一定温度下加热后会恢复原来的形状。NiTi合金的主要特点是其特殊的性能,即形状记忆效应和超弹性行为,以及优异的耐腐蚀性、高强度、低弹性模量和生物相容性。由于其超弹性,镍钛类似于一些人体刚性组织,包括骨骼和肌腱,使其能够用于骨科,神经病学,心脏病学,介入放射学,牙髓学等许多医疗病例的植入物或工具。本文研究了热处理对NiTi合金物理冶金性能的影响。在850℃固溶处理后,在450℃时效处理,得到了镍含量为50.6 (% Ni)、钛含量为49.4 (% Ti)的NiTi合金。用光学显微镜或扫描电镜观察了接收、固溶、固溶和时效阶段的显微组织。采用维氏显微硬度测定和差示扫描量热法分析热处理对合金显微组织和相变温度的影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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