Full-Field Deformation and Thermal Characterization of GNP/Epoxy and GNP/SMA Fiber/Epoxy Composites

Ugur Kilic, M. Sherif, S. Daghash, O. Ozbulut
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Abstract

Shape memory alloys (SMAs) are a class of metallic alloys that possess remarkable characteristics such as superelasticity and shape memory effect. Superelastic SMAs have been considered as fiber in polymer composites due to their ability to recover their deformation upon removal of load, good energy dissipation capacity and impact resistance. Graphene nanoplatelets (GNPs) consists of small stacks of graphene sheets that are two-dimensional. Both sides of atomic lattice of GNPs contact matrix of a composite system and can generate more sites for potential chemical and physical bonding with the host material. Most importantly, graphene sheets and their derivatives can be produced at large-scale for industrial demand at low-cost. This study explores the fabrication of multi-scale reinforced epoxy matrix composites in which GNPs and SMA strands are employed as nano- and micro-scale reinforcements, respectively. First, GNPs are dispersed into a ductile and brittle epoxy matrix to produce GNP/epoxy nanocomposites. To study the effect of GNP content on the behavior of the developed nanocomposite, GNPs are added to the epoxy-hardener mixture at different weight percentages (neat, 0.1%, 0.25%, 0.5%, 1%, and 2%). Uniaxial tensile tests of the developed nanocomposites are conducted under monotonic load up to failure. The optimum GNP content for GNP-reinforced epoxy matrix is determined and used in the fabrication of SMA fiber/epoxy composite. The developed multiscale reinforced epoxy composites are tested under tensile loading and their full-field strain and temperature behavior are monitored and evaluated using a digital image correlation system and an infrared thermal camera.
GNP/环氧树脂和GNP/SMA纤维/环氧复合材料的全场变形和热特性
形状记忆合金是一类具有超弹性和形状记忆效应的金属合金。超弹性sma具有在载荷解除后恢复变形的能力、良好的能量耗散能力和抗冲击性,被认为是聚合物复合材料中的一种纤维。石墨烯纳米片(GNPs)由二维石墨烯片的小堆组成。GNPs的原子晶格两侧接触复合体系的矩阵,可以产生更多的位点与主体材料进行潜在的化学和物理键合。最重要的是,石墨烯片及其衍生物可以以低成本大规模生产以满足工业需求。本研究探索了以GNPs和SMA分别作为纳米级和微级增强材料的多尺度增强环氧基复合材料的制备。首先,将GNPs分散到延展性和脆性的环氧基体中,以制备GNP/环氧纳米复合材料。为了研究GNP含量对制备的纳米复合材料行为的影响,将GNPs以不同的重量百分比(纯、0.1%、0.25%、0.5%、1%和2%)添加到环氧树脂-硬化剂混合物中。对所研制的纳米复合材料进行了单轴拉伸试验。确定了GNP增强环氧基的最佳GNP含量,并将其用于SMA纤维/环氧复合材料的制备。利用数字图像相关系统和红外热像仪对所研制的多尺度增强环氧复合材料进行了拉伸载荷试验,并对其全场应变和温度行为进行了监测和评价。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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