The Bioassay Guided Screening of Cryptolepis Extracts for Onward Synthesis of Nano Ferrites

Hafza Murtaza, Aasia Sikander, Umema Murtaza, A. Masroor, F. Ghafoor
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Abstract

In this study, various leaves and stem organic extracts were prepared using the solvents viz., n-hexane, ethyl acetate, ethanol and water, separately. Different phytochemical test for alkaloids, carbohydrates, oils, amino acids and others were performed to determine their presence in the extracts. These plant extracts were used for screening of sample via UV and HPLC techniques to compare the wavelength and absorbance, and retention time on chromatogram by extracts, respectively. The surface properties and size of nickel-zinc nano ferrites were evaluated by Energy-dispersive X-ray spectroscopy (EDX) and Scanning Electron Microscopy (SEM). The former, showed the presence of nickel (Ni) and zinc (Zn) weighing 4.27⁒ of N ,6.89⁒ of C and 35.5⁒ of O in the sample which confirmed the presence of nano ferrites in leaves and stem of C. buchanani.
用生物测定法筛选隐藻提取物制备纳米铁氧体
本研究分别以正己烷、乙酸乙酯、乙醇和水为溶剂制备了不同种类的叶茎有机提取物。对生物碱、碳水化合物、油脂、氨基酸等进行了不同的植物化学测试,以确定它们在提取物中的存在。利用紫外分光光度法和高效液相色谱法对样品进行筛选,比较提取液的波长、吸光度和色谱保留时间。利用能量色散x射线能谱(EDX)和扫描电子显微镜(SEM)对镍锌纳米铁氧体的表面性能和尺寸进行了表征。结果表明,样品中镍(Ni)和锌(Zn)含量分别为N的4.27⁒、C的6.89⁒和O的35.5⁒,证实了叶和茎中存在纳米铁氧体。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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