A new determination method of very low Fe contamination by UFS

Dian-Tong Lu, Zheng Qingcheng, I. V. Mitchell, P. Hemment, H. Ryssel
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Abstract

We have produced very low Fe-dose (10/sup 8/-10/sup 9/ Fe/cm/sup 2/) implanted Si samples. A new method of Ultraviolet Fluorescence Spectra (UFS) measurements has been used to determine the contents of Fe on the surfaces of Fe-implanted samples. We find that the Fe-impurities have their own ultraviolet fluorescent peak wavelength at room temperature and their characteristic spectral peak intensities are proportional to the Fe-doses (Fe-concentrations) in Fe implanted Si samples. This method is very sensitive, efficient and nondestructive for testing the Fe contamination on silicon. Some SOI (Silicon on Insulator) wafers and VLSI chips were evaluated with the UFS method. The results indicate that the UFS method is able to measure the very low Fe-contamination. The limit is below (10/sup 8/-10/sup 9/) Fe/cm/sup 2/ or (10/sup 13/-10/sup 14/) Fe/cm/sup 3/ in Si samples.
UFS法测定极低铁污染的新方法
我们已经生产了极低铁剂量(10/sup 8/-10/sup 9/ Fe/cm/sup 2/)的Si植入样品。采用紫外荧光光谱(UFS)法测定了注入铁样品表面铁的含量。我们发现,Fe杂质在室温下有自己的紫外荧光峰波长,其特征光谱峰强度与Fe注入Si样品中的Fe剂量(Fe浓度)成正比。该方法灵敏、高效、无损地检测了硅表面的铁污染。用UFS方法对一些绝缘体上硅(SOI)晶圆和VLSI芯片进行了评价。结果表明,UFS方法可以测量极低的铁污染。在Si样品中,极限低于(10/sup 8/-10/sup 9/) Fe/cm/sup 2/或(10/sup 13/-10/sup 14/) Fe/cm/sup 3/。
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