Morphological of Zinc Ferrite Nanostructure Using the Hydrothermal Synthesis

K. Lestari
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Abstract

Over the last two decades, many methods for synthesizing various ZnFe2O4 nanostructures of uniform size and shape, such as nanospheres, nanoflowers, nanorods, and nanotubes, have been developed. It seems challenging to investigate a practical and cost-effective method to synthesize cubic ZnFe2O4 magnetite with cubic morphological properties in an aqueous solution. The morphology of zinc ferrite nanostructures is mostly random and non-uniform. The objective of this study is to create reasonably uniform single-crystal zinc ferrite nanocubes. The hydrothermal method was used to successfully sample zinc ferrite by varying the amount of (En) ethylenediamine (0 - 2.4 mL) in the solution. The outcomes demonstrated that the nanocubes, with a particle size of nearly 48 nm, had a more uniform morphology than other samples. The morphology and dimensions of the samples were examined using scanning electron microscopy in conjunction with energy dispersion X-ray spectroscopy.
水热合成铁酸锌纳米结构的形貌研究
在过去的二十年里,人们开发了许多方法来合成各种尺寸和形状均匀的ZnFe2O4纳米结构,如纳米球、纳米花、纳米棒和纳米管。寻找一种在水溶液中合成具有立方形态的立方型ZnFe2O4磁铁矿的实用而经济的方法是一项具有挑战性的研究。铁酸锌纳米结构的形貌大多是随机的、不均匀的。本研究的目的是建立合理均匀的单晶铁氧体锌纳米立方体。水热法通过改变溶液中(En)乙二胺(0 ~ 2.4 mL)的量,成功地对铁氧体锌进行了取样。结果表明,粒径接近48 nm的纳米立方比其他样品具有更均匀的形貌。利用扫描电子显微镜结合能量色散x射线光谱学对样品的形貌和尺寸进行了检测。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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