Optical Characterization of Nickel Sulphide Thin Films Prepared by Chemical Bath Deposition Method

J. N. Nwauzor, E. Nnachi, I. S. Okoroudoh, M. Igbo, A. D. Babalola
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Abstract

Nickel sulfide thin films were prepared using chemical bath deposition method on a glass substrate. Nickel sulphate and sodium thiosulphate were used as starting chemicals. Ethylenediaminetetra-acetic acid (EDTA), was used as the complexing agent. In this study time was the only parameter optimized to get good quality thin film. Films were characterized using an UV M501 single beam scanning spectrophotometer from a wavelength of 220- 560nm. The nickel sulfide thin films exhibited direct band gap transition with band gap energy 2.3eV. A poor reflectance, moderate absorbance and high transmittance was recorded.
化学浴沉积法制备硫化镍薄膜的光学特性
采用化学浴沉积法在玻璃衬底上制备了硫化镍薄膜。用硫酸镍和硫代硫酸钠作为起始化学品。采用乙二胺四乙酸(EDTA)作为络合剂。在本研究中,时间是唯一优化得到高质量薄膜的参数。用紫外M501单光束扫描分光光度计在220 ~ 560nm波长范围内对薄膜进行了表征。硫化镍薄膜呈现直接带隙跃迁,带隙能达到2.3eV。具有较差的反射率、中等的吸光度和较高的透光率。
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