Features of the formation of highly sensitive nanoscale films SnO2 doped with platinum for sensing applications

K. Tsarik, V. Petukhov, N. S. Struchkov
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Abstract

In this work, we consider the formation of a sensor layer 100 nm thick based on platinum-doped tin oxide. We investigated the method of forming an oxide film using magnetron sputtering Sn and Pt in Ar+O2 plasma. Using X-ray diffraction, it was found that the film consists of nanoscale particles with a metal core. The average size of the nanoparticles forming the film was from 47 to 74 nm The characteristics of the film were measured during additional oxidation in the temperature range from 300 to 700 °C. Thanks to annealing, the resistance of the sensor layer can be varied from 10 kΩ to 100 MΩ at a detection temperature of 300 °C The optimized film has been tested to detect ethanol, acetone, and ammonia at streams of 50, 100, 150 ppm.
用于传感应用的高灵敏度SnO2掺杂铂纳米薄膜的形成特征
在这项工作中,我们考虑在铂掺杂氧化锡的基础上形成100 nm厚的传感器层。研究了在Ar+O2等离子体中磁控溅射Sn和Pt形成氧化膜的方法。利用x射线衍射,发现薄膜由具有金属核的纳米级颗粒组成。形成膜的纳米颗粒的平均尺寸为47 ~ 74 nm。在300 ~ 700℃的温度范围内进行额外氧化,测量了膜的特性。由于退火,传感器层的电阻可以在300°C的检测温度下从10 kΩ到100 MΩ变化。优化的薄膜已经测试了在50,100,150 ppm的流下检测乙醇,丙酮和氨。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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