Three-dimensional strategies in the quantitative resolution of kinetic UV absorbance measurements for monitoring the oxidation of quercetin by oxidant agents and analyzing dietary supplement product.

IF 2.6 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY
Erdal Dinç, Asiye Üçer, Nazangül Ünal
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引用次数: 2

Abstract

Three-dimensional strategies involving the application of parallel factor analysis (PARAFAC) to the kinetic UV absorbance measurements were elaborated to monitor the oxidation of quercetin with oxidant agents (K2Cr2O7 and KIO3) and to quantify analyte in a dietary supplement product. Loadings (spectral, kinetic and concentration profiles) were obtained by the PARAFAC deconvolution. Spectral identification, kinetics and quantification of the relevant analyte in the presence of interferent(s) were performed. The elaborated chemometric strategies were carefully validated to demonstrate the capability of the method. Assay results of the PARAFAC strategies were statistically compared to that of the newly developed UPLC method.

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槲皮素被氧化剂氧化和膳食补充剂产品分析中动态紫外吸收测量定量分辨的三维策略。
应用平行因子分析(PARAFAC)对动态紫外吸光度测量的三维策略进行了阐述,以监测槲皮素与氧化剂(K2Cr2O7和KIO3)的氧化,并定量分析膳食补充剂产品中的分析物。负载(光谱、动力学和浓度剖面)通过PARAFAC反褶积得到。在存在干扰的情况下,对相关分析物进行了光谱鉴定、动力学和定量分析。精心设计的化学计量策略经过仔细验证,以证明该方法的能力。对新开发的UPLC法和PARAFAC法的检测结果进行了统计比较。
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来源期刊
Journal of Food and Drug Analysis
Journal of Food and Drug Analysis 医学-食品科技
CiteScore
6.30
自引率
2.80%
发文量
36
审稿时长
3.8 months
期刊介绍: The journal aims to provide an international platform for scientists, researchers and academicians to promote, share and discuss new findings, current issues, and developments in the different areas of food and drug analysis. The scope of the Journal includes analytical methodologies and biological activities in relation to food, drugs, cosmetics and traditional Chinese medicine, as well as related disciplines of topical interest to public health professionals.
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