Transition-Metal-Free Synthesis of a Densely Functionalized Benzodioxole Intermediate toward Lotiglipron

已完结 10 由小太阳发布于 2024/3/19 12:52:03

DOI:10.1021/acs.oprd.3c00472
作者：Jimmy Wang, James Clarke, Matthew Badland, Brian Broadbelt, Louise F. Dow, Harriet A. M. Fenton, Daniel A. Laity, Jinu S. Mathew, Emily K. Rose, Neringa Tamosiunaite, Steven J. R. Twiddle, Robert Walton
文献类型：期刊论文
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American Chemical Society (ACS)

Abstract：A decagram-scale preparation of the key intermediate (±)-2-(4-bromo-2-methylbenzo[d][1,3]dioxol-2-yl)-5-chloropyridine is described. Key steps involve a double nucleophilic substitution of 3

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