{"title":"l -天冬酰胺掺杂TGS晶体的形态变化","authors":"S. Kalainathan , M.Beatrice Margaret , T. Irusan","doi":"10.1016/S1463-0184(02)00006-0","DOIUrl":null,"url":null,"abstract":"<div><p><span>This paper discusses the growth and properties of Triglycine Sulphate Crystals (TGS) and with L-Asparagine. Doped single crystal<span> was grown by slow-cooling solution growth technique. TGS crystals with 10 wt% of L-Asparagine exhibited prominent morphological changes in the (101) and (001) planes. Lattice parameter values were determined by powder X-ray diffraction analysis. Incorporation of L-Asparagine in TGS crystals has been qualitatively estimated and confirmed by Fourier Transform Infrared (FTIR) spectra. </span></span>Micro hardness studies also performed for the pure and doped crystals. A morphology diagram is given.</p></div>","PeriodicalId":10766,"journal":{"name":"Crystal Engineering","volume":"5 1","pages":"Pages 71-78"},"PeriodicalIF":0.0000,"publicationDate":"2002-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S1463-0184(02)00006-0","citationCount":"10","resultStr":"{\"title\":\"Morphological changes of L-asparagine doped TGS crystal\",\"authors\":\"S. Kalainathan , M.Beatrice Margaret , T. Irusan\",\"doi\":\"10.1016/S1463-0184(02)00006-0\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p><span>This paper discusses the growth and properties of Triglycine Sulphate Crystals (TGS) and with L-Asparagine. Doped single crystal<span> was grown by slow-cooling solution growth technique. TGS crystals with 10 wt% of L-Asparagine exhibited prominent morphological changes in the (101) and (001) planes. Lattice parameter values were determined by powder X-ray diffraction analysis. Incorporation of L-Asparagine in TGS crystals has been qualitatively estimated and confirmed by Fourier Transform Infrared (FTIR) spectra. </span></span>Micro hardness studies also performed for the pure and doped crystals. A morphology diagram is given.</p></div>\",\"PeriodicalId\":10766,\"journal\":{\"name\":\"Crystal Engineering\",\"volume\":\"5 1\",\"pages\":\"Pages 71-78\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2002-03-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/S1463-0184(02)00006-0\",\"citationCount\":\"10\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Crystal Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1463018402000060\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Crystal Engineering","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1463018402000060","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 10
摘要
本文讨论了硫酸甘油三酯晶体(TGS)的生长及其与l -天冬酰胺的性质。采用慢冷溶液生长技术生长掺杂单晶。含10 wt% l -天冬酰胺的TGS晶体在(101)和(001)平面上表现出明显的形态变化。通过粉末x射线衍射分析确定晶格参数值。用傅里叶变换红外光谱(FTIR)定性估计并证实了l -天冬酰胺在TGS晶体中的掺入。对纯晶体和掺杂晶体进行了显微硬度研究。并给出了形貌图。
Morphological changes of L-asparagine doped TGS crystal
This paper discusses the growth and properties of Triglycine Sulphate Crystals (TGS) and with L-Asparagine. Doped single crystal was grown by slow-cooling solution growth technique. TGS crystals with 10 wt% of L-Asparagine exhibited prominent morphological changes in the (101) and (001) planes. Lattice parameter values were determined by powder X-ray diffraction analysis. Incorporation of L-Asparagine in TGS crystals has been qualitatively estimated and confirmed by Fourier Transform Infrared (FTIR) spectra. Micro hardness studies also performed for the pure and doped crystals. A morphology diagram is given.
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