多孔聚合物复合Cu-(TAC)与活性炭空果棕榈油吸附可溶性氨

Rissah Maulina, R. Selly, H. Nasution, Jasmidi Jasmidi, M. Zubir, Siti Rahmah, P. Faradilla
{"title":"多孔聚合物复合Cu-(TAC)与活性炭空果棕榈油吸附可溶性氨","authors":"Rissah Maulina, R. Selly, H. Nasution, Jasmidi Jasmidi, M. Zubir, Siti Rahmah, P. Faradilla","doi":"10.24114/ijcst.v6i2.49375","DOIUrl":null,"url":null,"abstract":"This study aims to determine the stages in the process of making activated carbon, synthesis of porous polymer composites Cu(TAC) and activated carbon composites (KA-Cu(TAC) for adsorption of dissolved ammonia (NH4OH). To know the characterization results of activated carbon and KA- Cu(TAC), as well as knowing the optimum mass, concentration, and contact time of activated carbon KA-Cu(TAC) for the adsorption of dissolved ammonia. The research stages started from Empty Oil Palm Bunches (EFB) used as biosorbents for carbon production at 500oC. The resulting product was activated with H3PO4, then modified with porous polymer Cu(TAC) to make a composite. The KA-Cu(TAC) composite was synthesized by reflux method. Then MOFs, activated carbon and KACu(TAC) composite were characterized by BET. The BET characterization results showed that the successfully synthesized KA-Cu(TAC) composite experienced an increase in surface area.In the NH4OH adsorption process the optimum mass efficiency on activated carbon still increased at 8 grams while the KA-Cu(TAC) composite obtained an efficiency of 36, 6% and optimally at a mass of 4 g. At variations in concentration, the efficiency of the two samples still decreased. And the optimum time efficiency obtained in the NH4OH adsorption process with activated carbon was 70% and the KA-Cu(TAC) composite was 86.6%, both samples were equally optimal at 75 minutes.","PeriodicalId":13519,"journal":{"name":"Indonesian Journal of Chemical Science and Technology (IJCST)","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Adsorption Of Soluble Ammoniac Using A Porous Polymer Composite Cu-(TAC) And Activated Carbon Empty Fruit Palm Oil\",\"authors\":\"Rissah Maulina, R. Selly, H. Nasution, Jasmidi Jasmidi, M. Zubir, Siti Rahmah, P. Faradilla\",\"doi\":\"10.24114/ijcst.v6i2.49375\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study aims to determine the stages in the process of making activated carbon, synthesis of porous polymer composites Cu(TAC) and activated carbon composites (KA-Cu(TAC) for adsorption of dissolved ammonia (NH4OH). To know the characterization results of activated carbon and KA- Cu(TAC), as well as knowing the optimum mass, concentration, and contact time of activated carbon KA-Cu(TAC) for the adsorption of dissolved ammonia. The research stages started from Empty Oil Palm Bunches (EFB) used as biosorbents for carbon production at 500oC. The resulting product was activated with H3PO4, then modified with porous polymer Cu(TAC) to make a composite. The KA-Cu(TAC) composite was synthesized by reflux method. Then MOFs, activated carbon and KACu(TAC) composite were characterized by BET. The BET characterization results showed that the successfully synthesized KA-Cu(TAC) composite experienced an increase in surface area.In the NH4OH adsorption process the optimum mass efficiency on activated carbon still increased at 8 grams while the KA-Cu(TAC) composite obtained an efficiency of 36, 6% and optimally at a mass of 4 g. At variations in concentration, the efficiency of the two samples still decreased. And the optimum time efficiency obtained in the NH4OH adsorption process with activated carbon was 70% and the KA-Cu(TAC) composite was 86.6%, both samples were equally optimal at 75 minutes.\",\"PeriodicalId\":13519,\"journal\":{\"name\":\"Indonesian Journal of Chemical Science and Technology (IJCST)\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-07-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Indonesian Journal of Chemical Science and Technology (IJCST)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.24114/ijcst.v6i2.49375\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indonesian Journal of Chemical Science and Technology (IJCST)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.24114/ijcst.v6i2.49375","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

本研究旨在确定活性炭制备过程中的各个阶段,合成多孔聚合物复合材料Cu(TAC)和吸附溶解氨(NH4OH)的活性炭复合材料KA-Cu(TAC)。了解活性炭和KA-Cu(TAC)的表征结果,了解活性炭KA-Cu(TAC)吸附溶解氨的最佳质量、浓度和接触时间。研究阶段从空油棕束(EFB)作为生物吸附剂在500℃下生产碳开始。将所得产物用H3PO4活化,再用多孔聚合物Cu(TAC)进行改性制备复合材料。采用回流法制备了KA-Cu(TAC)复合材料。然后用BET对MOFs、活性炭和KACu(TAC)复合材料进行表征。BET表征结果表明,成功合成的KA-Cu(TAC)复合材料的表面积有所增加。活性炭吸附NH4OH的最佳质量效率在8 g时仍有提高,而KA-Cu(TAC)复合材料吸附NH4OH的最佳质量效率在4 g时达到36.6%。在浓度变化时,两种样品的效率仍然下降。活性炭吸附NH4OH的最佳时间效率为70%,KA-Cu(TAC)复合材料吸附NH4OH的最佳时间效率为86.6%,两种样品在75 min时同样最佳。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Adsorption Of Soluble Ammoniac Using A Porous Polymer Composite Cu-(TAC) And Activated Carbon Empty Fruit Palm Oil
This study aims to determine the stages in the process of making activated carbon, synthesis of porous polymer composites Cu(TAC) and activated carbon composites (KA-Cu(TAC) for adsorption of dissolved ammonia (NH4OH). To know the characterization results of activated carbon and KA- Cu(TAC), as well as knowing the optimum mass, concentration, and contact time of activated carbon KA-Cu(TAC) for the adsorption of dissolved ammonia. The research stages started from Empty Oil Palm Bunches (EFB) used as biosorbents for carbon production at 500oC. The resulting product was activated with H3PO4, then modified with porous polymer Cu(TAC) to make a composite. The KA-Cu(TAC) composite was synthesized by reflux method. Then MOFs, activated carbon and KACu(TAC) composite were characterized by BET. The BET characterization results showed that the successfully synthesized KA-Cu(TAC) composite experienced an increase in surface area.In the NH4OH adsorption process the optimum mass efficiency on activated carbon still increased at 8 grams while the KA-Cu(TAC) composite obtained an efficiency of 36, 6% and optimally at a mass of 4 g. At variations in concentration, the efficiency of the two samples still decreased. And the optimum time efficiency obtained in the NH4OH adsorption process with activated carbon was 70% and the KA-Cu(TAC) composite was 86.6%, both samples were equally optimal at 75 minutes.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信