表面功能化铁氧体锌纳米颗粒的结构、磁性和感应加热性能研究

Sandeep B. Somvanshi, R. V. Kumar, J. S. Kounsalye, T. Saraf, K. M. Jadhav
{"title":"表面功能化铁氧体锌纳米颗粒的结构、磁性和感应加热性能研究","authors":"Sandeep B. Somvanshi, R. V. Kumar, J. S. Kounsalye, T. Saraf, K. M. Jadhav","doi":"10.1063/1.5113361","DOIUrl":null,"url":null,"abstract":"In the present work, investigations of structural, magnetic and induction heating properties of surface functionalized zinc ferrite nanoparticles were carried out successfully. The zinc ferrite nanoparticles were prepared by co-precipitation route and further functionalized with oleic acid. The room temperature X-ray diffraction pattern confirmed the typical cubic spinel structure of the prepared nanoparticles. The average crystallite size calculated from Scherrer’s formula was found to be 12.30 nm confirming the nanocrystalline nature of zinc ferrite nanoparticles. The characteristic peaks observed in FT-IR spectrum confirmed the formation of cubic spinel structure and oleic acid coating over zinc ferrite nanoparticles. The room temperature magnetization behaviour revealed the superparamagnetic nature of the prepared nanoparticles. The induction heating behaviour shows a desirable amount (6 mg/mL) of zinc ferrite nanoparticles can able to achieve 42°C temperature for 600 s at 4.0 kA/m. This indicates that the resulting zinc ferrite nanoparticles are promising materials in magnetic hyperthermia treatments.","PeriodicalId":10874,"journal":{"name":"DAE SOLID STATE PHYSICS SYMPOSIUM 2018","volume":"1 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-07-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"52","resultStr":"{\"title\":\"Investigations of structural, magnetic and induction heating properties of surface functionalized zinc ferrite nanoparticles for hyperthermia applications\",\"authors\":\"Sandeep B. Somvanshi, R. V. Kumar, J. S. Kounsalye, T. Saraf, K. M. Jadhav\",\"doi\":\"10.1063/1.5113361\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In the present work, investigations of structural, magnetic and induction heating properties of surface functionalized zinc ferrite nanoparticles were carried out successfully. The zinc ferrite nanoparticles were prepared by co-precipitation route and further functionalized with oleic acid. The room temperature X-ray diffraction pattern confirmed the typical cubic spinel structure of the prepared nanoparticles. The average crystallite size calculated from Scherrer’s formula was found to be 12.30 nm confirming the nanocrystalline nature of zinc ferrite nanoparticles. The characteristic peaks observed in FT-IR spectrum confirmed the formation of cubic spinel structure and oleic acid coating over zinc ferrite nanoparticles. The room temperature magnetization behaviour revealed the superparamagnetic nature of the prepared nanoparticles. The induction heating behaviour shows a desirable amount (6 mg/mL) of zinc ferrite nanoparticles can able to achieve 42°C temperature for 600 s at 4.0 kA/m. This indicates that the resulting zinc ferrite nanoparticles are promising materials in magnetic hyperthermia treatments.\",\"PeriodicalId\":10874,\"journal\":{\"name\":\"DAE SOLID STATE PHYSICS SYMPOSIUM 2018\",\"volume\":\"1 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-07-12\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"52\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"DAE SOLID STATE PHYSICS SYMPOSIUM 2018\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1063/1.5113361\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"DAE SOLID STATE PHYSICS SYMPOSIUM 2018","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/1.5113361","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 52

摘要

本文成功地研究了表面功能化铁酸锌纳米颗粒的结构、磁性和感应加热性能。采用共沉淀法制备了铁酸锌纳米颗粒,并用油酸进一步功能化。室温x射线衍射图证实了制备的纳米颗粒具有典型的立方尖晶石结构。根据Scherrer公式计算得到的平均晶粒尺寸为12.30 nm,证实了铁酸锌纳米颗粒的纳米晶性质。红外光谱特征峰证实了铁酸锌纳米颗粒表面形成立方尖晶石结构和油酸涂层。室温磁化性能表明制备的纳米颗粒具有超顺磁性。感应加热行为表明,理想量(6 mg/mL)的铁酸锌纳米颗粒可以在4.0 kA/m下达到42°C温度600 s。这表明所得的铁酸锌纳米颗粒在磁热疗治疗中是有前途的材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Investigations of structural, magnetic and induction heating properties of surface functionalized zinc ferrite nanoparticles for hyperthermia applications
In the present work, investigations of structural, magnetic and induction heating properties of surface functionalized zinc ferrite nanoparticles were carried out successfully. The zinc ferrite nanoparticles were prepared by co-precipitation route and further functionalized with oleic acid. The room temperature X-ray diffraction pattern confirmed the typical cubic spinel structure of the prepared nanoparticles. The average crystallite size calculated from Scherrer’s formula was found to be 12.30 nm confirming the nanocrystalline nature of zinc ferrite nanoparticles. The characteristic peaks observed in FT-IR spectrum confirmed the formation of cubic spinel structure and oleic acid coating over zinc ferrite nanoparticles. The room temperature magnetization behaviour revealed the superparamagnetic nature of the prepared nanoparticles. The induction heating behaviour shows a desirable amount (6 mg/mL) of zinc ferrite nanoparticles can able to achieve 42°C temperature for 600 s at 4.0 kA/m. This indicates that the resulting zinc ferrite nanoparticles are promising materials in magnetic hyperthermia treatments.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信