采用机械合金化和放电等离子烧结技术合成了氮化钛增强铜基复合材料

Aleksandra Franczak, J. Karwan-Baczewska, D.Sc. Ph.D. Eng
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引用次数: 8

摘要

近年来,含有碳化物、硼化物或氮化物等陶瓷颗粒的铜基复合材料引起了人们的广泛关注。人们对这类材料越来越感兴趣,主要是因为它们具有高导电性和导热性、良好的机械和摩擦学性能以及微观结构的稳定性。在其他氮化物中,氮化钛似乎被认为是一种有吸引力的增强材料,因为它具有高硬度、优异的导电性和高温稳定性。此外,其良好的耐腐蚀性证明了TiN颗粒优于其他氮化物的独特性。本文采用机械合金化法制备了cu - 10wt .% TiN复合粉末,并采用火花等离子烧结技术在不同温度下烧结。采用扫描电镜(SEM)对所有粉末样品进行了机械合成后的形貌和粉末粒度的观察;同时进行了化学成分分析(EDS)。采用流体静力法测定了复合材料试样的密度,分析了制粉时间对复合粉末固结过程的影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
COPPER MATRIX COMPOSITES REINFORCED WITH TITANIUM NITRIDE PARTICLES SYNTHESIZED BY MECHANICAL ALLOYING AND SPARK PLASMA SINTERING
Copper matrix composites containing ceramic particles such as carbides, borides, or nitrides have attracted much attention over the last few years. The increased interest in such materials has mainly been created by their high electrical and thermal conductivity, good mechanical and tribological properties, and microstructural stability. Among other nitrides, the titanium nitride seems to be considered asan attractive reinforcement due to its high hardness, excellent electrical conductivity, and stability at high temperatures. Moreover, its good corrosion resistance proves the uniqueness of the TiN particles above any other nitrides. In this work, Cu-10 wt.% TiN composite powders were produced by mechanical alloying and sintered by the spark plasma sintering (SPS) technique under different temperatures. The morphology and powder particle size after mechanical synthesis were inspected by a scanning electron microscopy (SEM) for all of the powder samples; chemical composition analyses (EDS) were also  performed. The hydrostatic method was used to measure the density of the composite samples to analyze the influence of milling time on the process of consolidation in the composite powders.
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