氧化锆锂硅酸盐玻璃陶瓷抛光与釉烧试样的双轴抗折强度及微观结构比较

Alaa M. Attaallah, E. Zayed, Salma M Dabees, Youssef Y. Ashour, A. Fahmy
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引用次数: 2

摘要

玻璃陶瓷系统具有良好的美观性、高抗断裂性、粘合耐久性和使用CAD/CAM简化的制造技术,人们对其越来越感兴趣。本研究的目的是比较“抛光”和“釉质和烧制”硅酸锆锂(ZLS) CAD/CAM块Celtra Duo的抗弯强度。方法:选取14只德国Dentsply Sirona的Celtra Duo标本,平均分为两组,第一组(n=7;第二组(n=7;根据制造商的说明进行上釉和烧制。然后在抛光、上釉、烧成后,采用通用试验机和活塞-三球法,按照ISO 6872进行双轴抗折强度测试。采用扫描电镜(Jeol/GSM5300)观察断口形貌和显微组织。采用SPSS 20.0软件对数据进行统计学分析。结果:抛光后的ZLS玻璃陶瓷盘与釉面烧制后的ZLS玻璃陶瓷盘双轴抗折强度差异有统计学意义,抛光后的ZLS玻璃陶瓷盘双轴抗折强度较抛光后的ZLS玻璃陶瓷盘低(平均±标准差:158.7±21.67 MPa),釉面陶瓷盘双轴抗折强度较高(平均±标准差:261.5±31.89 MPa)。结论:与抛光相比,上釉和烧成明显提高了Celtra Duo样品的双轴抗折强度,但微观结构没有明显变化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Comparison between Biaxial Flexural Strength and Microstructure of Polished and Glaze-Fired Specimens of Zirconia Lithium Silicate Glass Ceramic
Introduction: There has been a growing interest in glass ceramic systems with good esthetics, high fracture resistance, bonding durability, and simplified fabrication techniques using CAD/CAM. The aim of this study was to compare flexural strength in "polished" and "glazed and fired" specimens of zirconium lithium silicate (ZLS) CAD/CAM blocks Celtra Duo. Methods: A total of 14 specimens of Celtra Duo (Dentsply Sirona, Germany) were designated and equally divided into two groups, including group I (n=7; as polished) and group II (n=7; as glazed and fired) according to the manufacturers’ instructions. Then biaxial flexural strength was tested according to ISO 6872 using a universal testing machine and piston-on-three-ball method after polishing, glazing, and firing. The fractured surfaces and microstructure were observed by scanning electron microscope (Jeol/GSM5300). Data were then statistically analyzed using SPSS software (version 20.0). Results: There were statistically significant differences in biaxial flexural strength between a polished and glaze-fired specimen of ZLS glass ceramic discs as biaxial flexural strength was lower in polished specimens (mean±standard deviation: 158.7±21.67 MPa), while the glazed specimens showed higher biaxial flexural strength (mean±standard deviation: 261.5±31.89 MPa). Conclusion: Glazing and firing of Celtra Duo specimens increased biaxial flexural strength significantly in comparison to polishing with no significant change in the microstructure.
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