Chuyên Thuận Nguyễn, Chanthana Susawaengsup, Thomas Singer, Krittiya Tongkoom, Ralf Oberg, Rapeephun Dangtungee, P. Bhuyar
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引用次数: 1
摘要
沉香油是中东和海湾国家香水工业中必不可少的生物活性物质之一。内置的功能和可用的生物活性成分的油使沉香更加珍贵。本研究采用微波辅助索氏提取法提取物理诱导的沉香木屑。采用气相色谱-质谱联用(GCMS) (Agilent GC 6890zN MS 5973)对提取的油样与未感染的对照进行分析。微波辅助索氏提取法可获得较高的油提取率。在物理诱导的样品中,用GC-MS记录了24个信号峰。记录到的峰面积最突出的是-5-羟基-3-甲基-1-吲哚酮,在41.89 min检测到,峰面积为17.64%,其次是-甲基4,4,7-三甲基4.7-二氢吲哚-6-羧酸酯,在23.17 min检测到,峰面积为15.54%;紧随其后的是3-carene,用时46.61分钟。研究结果表明,微波辅助索氏提取法在沉香工业中具有较好的优势,可用于提高沉香油的产量。
Gas chromatography analysis of the microwave-aided extracted agarwood oil from physically induced Aquilaria malaccensis trees in Northern Thailand
Agarwood (Aquilaria malaccensis) oil is one of the essential bioactive materials in the scent/ perfume industry for the middle east and gulf countries. The built-in functionality and availability of bioactive components of oil make agarwood more precious. In this study, the physically induced infected agarwood tree chops were extracted by microwave assisted Soxhlet extraction. Moreover, the extracted oil samples were analyzed against control not infected trees using Gas chromatography-mass spectroscopy (GC-MS) by GCMS (Agilent GC 6890zN MS 5973). The microwave assisted Soxhlet extraction revealed a higher amount of oil extraction. In the physically induced samples, 24 signal peaks were recorded employing GC-MS. The most prominent peak area recorded was -5-hydroxy-3-methyl-1-indanone detected at minute 41.89 with a peak area of 17.64%, followed by -methyl 4,4,7-trimethyl 4.7-dihydro indan -6- carboxylate at 23.17 min, occupying an area of 15.54%; followed by 3-carene recorded at 46.61 minutes with an area. According to this research, the microwave-assisted Soxhlet extraction method outperformed and can be utilized in the agarwood industry for enhanced oil production.