Y D G Edañol, K. Usman, Jr. C. Buenviaje Salvador, Michael E. Mantua, Jr. M. Payawan Leon
{"title":"利用稻壳二氧化硅水热合成Y型沸石","authors":"Y D G Edañol, K. Usman, Jr. C. Buenviaje Salvador, Michael E. Mantua, Jr. M. Payawan Leon","doi":"10.26534/KIMIKA.V29I1.17-21","DOIUrl":null,"url":null,"abstract":"Rice hull, a known agricultural waste product, with 21% silica (SiO2) content based on elemental analysis, is a promising starting material for zeolite Y synthesis. In this work, silica derived from rice hull samples were extracted via alkaline treatment using 4M NaOH at 130 °C - 150 °C. Further introduction of NaOH and inclusion of aluminium hydroxide were done before subjecting the materials to subsequent ageing and heating at 95 °C to form the zeolite Y crystals. The samples were then analyzed using Fourier transform infrared spectroscopy (FT-IR) and X-ray diffractometry (XRD). Zeolite Y from commercial silica was also synthesized as negative control and together with commercially available zeolite Y, FT-IR and XRD results showed that they possess similar structures with the rice-hull derived material.","PeriodicalId":17914,"journal":{"name":"KIMIKA","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2018-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Utilizing Silica from Rice Hull for the Hydrothermal Synthesis of Zeolite Y\",\"authors\":\"Y D G Edañol, K. Usman, Jr. C. Buenviaje Salvador, Michael E. Mantua, Jr. M. Payawan Leon\",\"doi\":\"10.26534/KIMIKA.V29I1.17-21\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Rice hull, a known agricultural waste product, with 21% silica (SiO2) content based on elemental analysis, is a promising starting material for zeolite Y synthesis. In this work, silica derived from rice hull samples were extracted via alkaline treatment using 4M NaOH at 130 °C - 150 °C. Further introduction of NaOH and inclusion of aluminium hydroxide were done before subjecting the materials to subsequent ageing and heating at 95 °C to form the zeolite Y crystals. The samples were then analyzed using Fourier transform infrared spectroscopy (FT-IR) and X-ray diffractometry (XRD). Zeolite Y from commercial silica was also synthesized as negative control and together with commercially available zeolite Y, FT-IR and XRD results showed that they possess similar structures with the rice-hull derived material.\",\"PeriodicalId\":17914,\"journal\":{\"name\":\"KIMIKA\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-06-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"KIMIKA\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.26534/KIMIKA.V29I1.17-21\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"KIMIKA","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.26534/KIMIKA.V29I1.17-21","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Utilizing Silica from Rice Hull for the Hydrothermal Synthesis of Zeolite Y
Rice hull, a known agricultural waste product, with 21% silica (SiO2) content based on elemental analysis, is a promising starting material for zeolite Y synthesis. In this work, silica derived from rice hull samples were extracted via alkaline treatment using 4M NaOH at 130 °C - 150 °C. Further introduction of NaOH and inclusion of aluminium hydroxide were done before subjecting the materials to subsequent ageing and heating at 95 °C to form the zeolite Y crystals. The samples were then analyzed using Fourier transform infrared spectroscopy (FT-IR) and X-ray diffractometry (XRD). Zeolite Y from commercial silica was also synthesized as negative control and together with commercially available zeolite Y, FT-IR and XRD results showed that they possess similar structures with the rice-hull derived material.