Diels-Alder反应合成降冰片烯衍生物

Advanced Materials Research Pub Date : 2011-12-01 DOI:10.4028/www.scientific.net/AMR.421.136

J. Park, H. Oh, Y. Park, Je-Wan Woo

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引用次数: 7

摘要

环戊二烯是制备降冰片烯的重要原料，可通过马来酸酯和Diels-Alder反应合成降冰片烯二羧酸酯。并合成了与典型PVC增塑剂邻苯二甲酸二辛酯(DOP)相似的结构，通过1H-NMR、FT-IR、Mass、HPLC等手段确定了化合物的结构，并与DOP的基本性质进行了比较。

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Synthesis of Norbornene Derivative Using Diels-Alder Reaction

Cyclopentadiene is an important material for making norbornene, and can synthesize norbornene dicarboxylic ester through the maleate and Diels-Alder reaction. Also, a structure similar to that of the representative PVC plasticizer dioctyl phthalate(DOP) was synthesized, so as to confirm the structure of compounds through 1H-NMR, FT-IR, Mass, and HPLC, and to compare the basic properties with those of DOP.

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Advanced Materials Research

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