光催化材料srfix - 1fexo3 (x= 0、0.05、0.1、0.15、0.2)的熔盐合成

A. D. Prasetiyo, D. R. Novianti, Hasal Maulidianingtiyas, A. Prasetyo
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引用次数: 0

摘要

SrTiO3是一种具有钙钛矿型结构的材料,因其在压电、光催化等领域具有广泛的应用前景而备受关注。SrTiO3光催化剂材料的带隙能为3.2 eV,工作波长为387.45 nm(紫外光)。据报道,金属掺杂SrTiO3能降低其带隙能。在本研究中,我们采用熔盐法合成了铁掺杂的SrTiO3 (SrTix-1FexO3(x= 0,0.05, 0.1, 0.15, 0.2))。SrTix-1FexO3(x= 0、0.05、0.1、0.15、0.2)的衍射图显示,样品目标成功合成,但在x= 0.2处仍发现杂质(TiO2相)。SEM图像显示,掺杂铁的SrTiO3颗粒形貌呈立方状,且存在团聚现象。紫外-可见DRS光谱分析表明,铁掺杂能显示出可见光区的光吸收。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Molten salt synthesis of photocatalyst material SrTix-1FexO3 (x= 0, 0.05, 0.1, 0.15, and 0.2)
SrTiO3 is a material with perovskite-type structure which received many attentions because it has a wide potential in various fields such as piezoelectric and photocatalyst. The photocatalyst material of SrTiO3 have band gap energy 3.2 eV, as results it will work on wavelength 387.45 nm (ultraviolet light). Doping metal to SrTiO3 was reported to decrease its band gap energy. In this research, we synthesized iron-doped SrTiO3 (SrTix-1FexO3(x= 0, 0.05, 0.1, 0.15, and 0.2)) using molten salt method. The diffractogram of SrTix-1FexO3(x= 0, 0.05, 0.1, 0.15, and 0.2) showed that the samples goal were successfully synthesized, but still found impurities (TiO2 phase) at x= 0.2. The SEM images showed that the morphology of particles is cubic and there are found agglomeration in iron-doped SrTiO3. The UV-Vis DRS spectra showed that iron dopant can reveal the light absorption in visible wavelength region.
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