以改性棉纱和油棕干纤维为原料,乳液法制备纤维素微球

Malaysian Journal, Fabrikasi Mikrosfera Selulosa, daripada Linter, Kapas dan Gentian Batang, Kelapa Sawit, Termodifikasi Melalui, Kaedah Emulsi, Nurul Shuhadah Mahadi, M. Nizam, S. Zakaria, M. F. Daud, Sharifah Nabihah Syed Jaafar
{"title":"以改性棉纱和油棕干纤维为原料,乳液法制备纤维素微球","authors":"Malaysian Journal, Fabrikasi Mikrosfera Selulosa, daripada Linter, Kapas dan Gentian Batang, Kelapa Sawit, Termodifikasi Melalui, Kaedah Emulsi, Nurul Shuhadah Mahadi, M. Nizam, S. Zakaria, M. F. Daud, Sharifah Nabihah Syed Jaafar","doi":"10.17576/mjas-2018-2205-20","DOIUrl":null,"url":null,"abstract":"In this study, cellulose microspheres from modified cotton linter (CL) and oil palm trunk fibre (OPTF) were fabricated by using simple emulsion method. The cellulose was obtained from the CL and OPTF through the alkaline pre-treatment and acid hydrolysis processes. The emulsion method was performed using polyvinyl alcohol (PVA) as an emulsifying agent. The characterization of the cellulose from CL and OPTF were analysed using Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD), and the morphological characterizations of cellulose microspheres were later observed under optical microscopy (OM) and field emission-scanning electron microscopy (FE-SEM). Based on the results, FTIR spectra displayed the lignin and hemicellulose had removed after treatments, while XRD revealed that the crystallinity index of OPTF and CL was increased after the treatments. The microspheres, formed with different ranges of size between 80 to 150 μm under OM and FESEM, showed the formation of pores on the surface of the microspheres.","PeriodicalId":18025,"journal":{"name":"Malaysian Journal of Analytical Science","volume":"25 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2018-10-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"FABRICATION OF CELLULOSE MICROSPHERES FROM MODIFIED COTTON LINTER AND OIL PALM TRUNK FIBRE VIA EMULSION METHOD\",\"authors\":\"Malaysian Journal, Fabrikasi Mikrosfera Selulosa, daripada Linter, Kapas dan Gentian Batang, Kelapa Sawit, Termodifikasi Melalui, Kaedah Emulsi, Nurul Shuhadah Mahadi, M. Nizam, S. Zakaria, M. F. Daud, Sharifah Nabihah Syed Jaafar\",\"doi\":\"10.17576/mjas-2018-2205-20\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, cellulose microspheres from modified cotton linter (CL) and oil palm trunk fibre (OPTF) were fabricated by using simple emulsion method. The cellulose was obtained from the CL and OPTF through the alkaline pre-treatment and acid hydrolysis processes. The emulsion method was performed using polyvinyl alcohol (PVA) as an emulsifying agent. The characterization of the cellulose from CL and OPTF were analysed using Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD), and the morphological characterizations of cellulose microspheres were later observed under optical microscopy (OM) and field emission-scanning electron microscopy (FE-SEM). Based on the results, FTIR spectra displayed the lignin and hemicellulose had removed after treatments, while XRD revealed that the crystallinity index of OPTF and CL was increased after the treatments. The microspheres, formed with different ranges of size between 80 to 150 μm under OM and FESEM, showed the formation of pores on the surface of the microspheres.\",\"PeriodicalId\":18025,\"journal\":{\"name\":\"Malaysian Journal of Analytical Science\",\"volume\":\"25 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-10-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Malaysian Journal of Analytical Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.17576/mjas-2018-2205-20\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Malaysian Journal of Analytical Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17576/mjas-2018-2205-20","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

以改性棉絮(CL)和油棕榈干纤维(OPTF)为原料,采用简单乳化法制备纤维素微球。通过碱前处理和酸水解得到纤维素。以聚乙烯醇(PVA)为乳化剂,进行了乳化法。利用傅里叶红外光谱(FTIR)和x射线衍射(XRD)对CL和OPTF制备的纤维素进行了表征,并在光学显微镜(OM)和场发射扫描电镜(FE-SEM)下观察了纤维素微球的形态特征。结果表明,FTIR光谱显示处理后木质素和半纤维素被去除,而XRD显示处理后OPTF和CL的结晶度指数有所提高。在OM和FESEM下形成的微球尺寸在80 ~ 150 μm之间,微球表面有孔洞形成。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
FABRICATION OF CELLULOSE MICROSPHERES FROM MODIFIED COTTON LINTER AND OIL PALM TRUNK FIBRE VIA EMULSION METHOD
In this study, cellulose microspheres from modified cotton linter (CL) and oil palm trunk fibre (OPTF) were fabricated by using simple emulsion method. The cellulose was obtained from the CL and OPTF through the alkaline pre-treatment and acid hydrolysis processes. The emulsion method was performed using polyvinyl alcohol (PVA) as an emulsifying agent. The characterization of the cellulose from CL and OPTF were analysed using Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD), and the morphological characterizations of cellulose microspheres were later observed under optical microscopy (OM) and field emission-scanning electron microscopy (FE-SEM). Based on the results, FTIR spectra displayed the lignin and hemicellulose had removed after treatments, while XRD revealed that the crystallinity index of OPTF and CL was increased after the treatments. The microspheres, formed with different ranges of size between 80 to 150 μm under OM and FESEM, showed the formation of pores on the surface of the microspheres.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信