纳米银的合成研究

Md. Ashraful Alam, Salma Akter Munni, Sabrina Mostafa, Raton Kumar Bishwas, S. Jahan
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引用次数: 1

摘要

纳米科学和纳米生物技术为探索杀菌和杀真菌活性提供了巨大的机会。自古以来,银就以其抗菌作用而闻名,几个世纪以来,它一直被用于预防和控制各种感染。对有效利用银纳米材料的合成和表征在现代科学中起着至关重要的作用。目的:我们的目标是制备银纳米材料,因为研究表明银纳米颗粒对细菌生物膜具有有效的活性。方法:一般采用溶胶-凝胶法在不同前驱体和螯合剂的存在下合成纳米银。结果:通过x射线衍射(XRD),得到米勒指数为(111)(200)(220)(311)(222)的立方晶胞,晶粒尺寸约为50.00nm。通过10.00 nm以下的扫描电镜和5.00nm以下的透射电镜对所制备的纳米颗粒的尺寸、形状、表面等进行了表征。DLS是一种独特的技术,可以识别约65.00nm的颗粒大小和纳米颗粒在水或生理溶液中的大小分布。结论:AgNPs与其他抗菌药物联合合成和使用的研究总体上有助于减少毒性问题,避免耐药性的产生,有力地增强了杀微生物效果。本文简要而精确地描述了无水SGM等纳米银的化学合成过程。此外,本文还简要介绍了纳米颗粒的不同表征技术,如x射线衍射,回顾了米勒指数(111)(200)(220)(311)(222)立方晶的晶体形状,其中晶粒尺寸约为50.00nm,制备的纳米颗粒的形貌通过扫描电镜显示为10.00nm。动态光散射表征了纳米材料在65.00nm左右的粒径,透射电镜表征了纳米材料的球形结构。进一步的研究将继续进行陶瓷涂层AgNPs的抗菌活性测试。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
An Investigation on Synthesis of Silver Nanoparticles
Introduction: Nano science and nano biotechnology provided enormous opportunities for exploring the bactericidal and fungicidal activities. Since ancient times, silver was known for its anti-bacterial effects and for centuries it has been used for prevention and control of disparate infections. On the effective use silver nanomaterials synthesized and characterized play a vital role of the modern science. Aims: Our goal is to prepare silver nanomaterials since studies have shown that silver nanoparticles have efficient activity against bacterial biofilms. Methodology: The silver nanoparticles were generally synthesized by non-aqueous sol-gel technique in the presence of different precursor by chelating agent. Results: Here found a cubic unit cell with miller indices (111) (200) (220) (311) (222) and crystallite size around 50.00nm by XRD. The morphology of the prepared nano particles has been revealed by SEM below 10.00 nm and TEM is below 5.00nm in size of graphical presentation such as size, shape, surface etc. of the nanoparticles. DLS is a unique technique to discern particle size around 65.00nm and size distributions in aqueous or physiological solutions of the nanoparticles. Conclusion: The studies on the combined synthesized and use of AgNPs with other antimicrobial agents generally help reduce the problem of toxicity and to avoid the potential for development of resistance and strongly enhance the microbicidal effect. This paper describes a short and very precise description about the chemical synthesis process of silver nanoparticles like no aqueous SGM. Also, this paper contains a brief description about different characterization technique of nanoparticles like X-ray Diffraction review the shape of crystal a cubic unit cell with miller indices (111) (200) (220) (311) (222) where crystallite size around 50.00nm, the morphology of the prepared nanoparticles has been revealed with size 10.00nm by SEM, Dynamic Light Scattering discern particle size around 65.00nm and Transmission Electron Microscope review the spherical shape of the nanomaterials.  Further investigation will be continuing the antimicrobial activity test of AgNPs with ceramic coating.
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