U. Ashiq, R. Jamal, M. Mahroof-Tahir, A. Keramidas, Z. Maqsood, K. Khan, M. Tahir
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引用次数: 4
摘要
合成了标题化合物，并通过x射线衍射分析确定了其晶体结构。该化合物为单斜晶，空间群P21/a, Z = 4。单元胞尺寸为a = 12.287(2) a, b = 3.8287(5) a, c = 16.0936(19) a， β = 97.409°，V = 750.77(19)A3。1223次反射的R值为0.0313。在结构中观察到N- h…O和N- h…N型分子间氢键。
The title compound was synthesized and its crystal structure was determined by X-ray diffraction analysis. The compound is monoclinic, space group P21/a with Z = 4. The unit-cell dimensions are a = 12.287(2)A, b = 3.8287(5)A, c = 16.0936(19)A, β = 97.409° and V = 750.77(19)A3. The R value is 0.0313 for 1223 observed reflections. Intermolecular hydrogen bonds of the type N-H…O and N-H…N were observed in the structure.
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