{"title":"抗结核候选物铁(III) 4-氟- n′-[(吡啶-4-基)羰基]苯并肼配合物的表征与合成","authors":"R. Ruswanto","doi":"10.36465/JOP.V1I2.332","DOIUrl":null,"url":null,"abstract":"<p><em>Synthesis of Fe (III) complex compounds with 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide ligand aims to find out the synthesis method, the complex and characteristic compound formulas of the complexes formed. Instruments used are UV-Visible Spectrophotometry, Infrared Spectrophotometry and Atomic Absorption Spectrophotometry. The synthesis of Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complexes can be synthesized by mixing metals and ligands dissolved in ethanol by heating at a temperature of 78oC. Compounds of synthesis can form complexes with the formula Fe(C<sub>13</sub>H<sub>10</sub>FN<sub>3</sub>O<sub>2</sub>)Cl<sub>3</sub>.2H<sub>2</sub>O. Characteristics of the Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complex compound have a maximum wavelength of 265.6 nm. The absorption of functional groups on the 540.0 cm-1 infra red wave spectrum</em><em>.</em><em></em></p><p><strong> </strong><strong><em>Keywords:</em></strong><strong><em> </em></strong><em>synthesis, complex, Fe (III), benzohydrazide</em></p><p> </p>","PeriodicalId":16805,"journal":{"name":"Journal of Pharmacopolium","volume":"129 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2018-08-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"CHARACTERIZATION AND SYNTHESIZE OF Fe(III) 4-FLUORO-N’-[(PYRIDINE-4-YL)CARBONYL]BENZOHYDRAZIDE COMPLEX AS ANTITUBERCULOSIS CANDIDATE\",\"authors\":\"R. Ruswanto\",\"doi\":\"10.36465/JOP.V1I2.332\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><em>Synthesis of Fe (III) complex compounds with 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide ligand aims to find out the synthesis method, the complex and characteristic compound formulas of the complexes formed. Instruments used are UV-Visible Spectrophotometry, Infrared Spectrophotometry and Atomic Absorption Spectrophotometry. The synthesis of Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complexes can be synthesized by mixing metals and ligands dissolved in ethanol by heating at a temperature of 78oC. Compounds of synthesis can form complexes with the formula Fe(C<sub>13</sub>H<sub>10</sub>FN<sub>3</sub>O<sub>2</sub>)Cl<sub>3</sub>.2H<sub>2</sub>O. Characteristics of the Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complex compound have a maximum wavelength of 265.6 nm. The absorption of functional groups on the 540.0 cm-1 infra red wave spectrum</em><em>.</em><em></em></p><p><strong> </strong><strong><em>Keywords:</em></strong><strong><em> </em></strong><em>synthesis, complex, Fe (III), benzohydrazide</em></p><p> </p>\",\"PeriodicalId\":16805,\"journal\":{\"name\":\"Journal of Pharmacopolium\",\"volume\":\"129 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-08-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Pharmacopolium\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.36465/JOP.V1I2.332\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Pharmacopolium","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.36465/JOP.V1I2.332","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
CHARACTERIZATION AND SYNTHESIZE OF Fe(III) 4-FLUORO-N’-[(PYRIDINE-4-YL)CARBONYL]BENZOHYDRAZIDE COMPLEX AS ANTITUBERCULOSIS CANDIDATE
Synthesis of Fe (III) complex compounds with 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide ligand aims to find out the synthesis method, the complex and characteristic compound formulas of the complexes formed. Instruments used are UV-Visible Spectrophotometry, Infrared Spectrophotometry and Atomic Absorption Spectrophotometry. The synthesis of Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complexes can be synthesized by mixing metals and ligands dissolved in ethanol by heating at a temperature of 78oC. Compounds of synthesis can form complexes with the formula Fe(C13H10FN3O2)Cl3.2H2O. Characteristics of the Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complex compound have a maximum wavelength of 265.6 nm. The absorption of functional groups on the 540.0 cm-1 infra red wave spectrum.
Keywords:synthesis, complex, Fe (III), benzohydrazide
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