席夫碱及乙二胺与1-苯基- 1,3 -丁二和4-氨基安替比林衍生的cr (Ii)、Fe (Ii)和Cd(Ii)配合物的合成与表征

University of Thi-Qar Journal Pub Date : 2019-04-25 DOI:10.32792/utq/utj/vol14/1/7

Israa Jirjees

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引用次数: 0

摘要

以1-苯基、1,3-丁二苯和4-氨基安替吡林与乙二胺反应合成席夫碱配体[(4Z,11aE,15E) -2,3,59,10 -五甲基-1,7,11-三苯基-2,6,10,11,13,14-六氢- 1h二吡唑[4,3-b:3'，4'-h][1,4,7,10]四氮杂环三叉星]。其配合物与Cr (II)、Fe (II)、Cd (II)等金属盐的配合物反应，通过元素分析、FT-IR、质谱技术和1h - nmr对配合物及其配体进行了表征

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Synthesis and Characterization of Schiffbases Andcr (Ii), Fe (Ii) and Cd(Ii) Complexes Derived From Ethelene Diammine With 1-Phenyl-1, 3-Butanedion and 4-Aminoantipyrine

Schiff base ligand [ (4Z,11aE,15E) -2,3,59,10 - pentamethyl -1,7,11-triphenyl-2,6,10,11,13,14-hexahydro -1H dipyrazol [4,3-b:3',4'-h][1,4,7,10] tetraazacyclotridecine ] was synthesized by reacting 1-Phenyl,1,3-butanedion and 4-aminoantipyrin with Ethylenediamine.Its complexes with Cr (II),Fe (II) and Cd (II) reaction of the metal salt with the ligand characterization ligands and its complexes were characterized by elements analyses , FT-IR , Mass techniques and 1 H-NMR

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University of Thi-Qar Journal

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