{"title":"原甘菊甲醇提取物化学成分分析(茄科)","authors":"Thi Thanh Thuy Tran, H. P. Dang, T. Nguyen","doi":"10.31276/vjste.61(3).09-11","DOIUrl":null,"url":null,"abstract":"Solanum procumbens L. (Solanaceae) were extracted respectively with n-hexane, ethyl acetate, and methanol to obtain the corresponding extracts. The methanol-soluble extract was acidified by adding HCl 0.5M; this was followed by liquid-liquid partition with CHCl3 to afford CHCl3-soluble fraction. From this fraction, four compounds were isolated and identified as ergosterol peroxide (1), 9,11-dehydroergosterol peroxide (2), N-(N-benzoyl-L-phenylalanyl)-L-phenylalanol (3), and moupinamide (4). Their structures were elucidated based on the NMR spectroscopic analysis and comparison with the literature. All isolated compounds were first reported from S. procumbens.","PeriodicalId":23548,"journal":{"name":"Vietnam Journal of Science, Technology and Engineering","volume":"16 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-09-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Chemical constituents from methanolic extract of Solanum procumbens Lour (Solanaceae)\",\"authors\":\"Thi Thanh Thuy Tran, H. P. Dang, T. Nguyen\",\"doi\":\"10.31276/vjste.61(3).09-11\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Solanum procumbens L. (Solanaceae) were extracted respectively with n-hexane, ethyl acetate, and methanol to obtain the corresponding extracts. The methanol-soluble extract was acidified by adding HCl 0.5M; this was followed by liquid-liquid partition with CHCl3 to afford CHCl3-soluble fraction. From this fraction, four compounds were isolated and identified as ergosterol peroxide (1), 9,11-dehydroergosterol peroxide (2), N-(N-benzoyl-L-phenylalanyl)-L-phenylalanol (3), and moupinamide (4). Their structures were elucidated based on the NMR spectroscopic analysis and comparison with the literature. All isolated compounds were first reported from S. procumbens.\",\"PeriodicalId\":23548,\"journal\":{\"name\":\"Vietnam Journal of Science, Technology and Engineering\",\"volume\":\"16 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-09-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Vietnam Journal of Science, Technology and Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.31276/vjste.61(3).09-11\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Vietnam Journal of Science, Technology and Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.31276/vjste.61(3).09-11","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Chemical constituents from methanolic extract of Solanum procumbens Lour (Solanaceae)
Solanum procumbens L. (Solanaceae) were extracted respectively with n-hexane, ethyl acetate, and methanol to obtain the corresponding extracts. The methanol-soluble extract was acidified by adding HCl 0.5M; this was followed by liquid-liquid partition with CHCl3 to afford CHCl3-soluble fraction. From this fraction, four compounds were isolated and identified as ergosterol peroxide (1), 9,11-dehydroergosterol peroxide (2), N-(N-benzoyl-L-phenylalanyl)-L-phenylalanol (3), and moupinamide (4). Their structures were elucidated based on the NMR spectroscopic analysis and comparison with the literature. All isolated compounds were first reported from S. procumbens.