维生素c对电抛光钢形貌和光学性能的影响

F. Abouzeid
{"title":"维生素c对电抛光钢形貌和光学性能的影响","authors":"F. Abouzeid","doi":"10.5897/AJPAC2015.0631","DOIUrl":null,"url":null,"abstract":"The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations. \n \n   \n \n Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.","PeriodicalId":7556,"journal":{"name":"African Journal of Pure and Applied Chemistry","volume":"67 1","pages":"135-145"},"PeriodicalIF":0.0000,"publicationDate":"2015-06-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A study of the morphology and optical properties of electro polished steel in the presence of Vitamin-C\",\"authors\":\"F. Abouzeid\",\"doi\":\"10.5897/AJPAC2015.0631\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations. \\n \\n   \\n \\n Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.\",\"PeriodicalId\":7556,\"journal\":{\"name\":\"African Journal of Pure and Applied Chemistry\",\"volume\":\"67 1\",\"pages\":\"135-145\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2015-06-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"African Journal of Pure and Applied Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5897/AJPAC2015.0631\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"African Journal of Pure and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5897/AJPAC2015.0631","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

采用动电位极化法研究了钢在正磷酸中的电化学抛光过程。电解抛光在含有维生素C的溶液中进行。在电解抛光溶液中加入维生素C可以降低极限电流。建立了维生素C浓度对电抛光过程和表面织构的影响(AFM, SEM)和UV-VIS-NIR光谱。结果表明:随着维生素C浓度从2 × 10-5增加到5 × 10-5 M,钢试样的粗糙度和反射率分别减小和增大;当浓度增加到10 × 10-5 M时,则出现相反的趋势。电抛光前钢试样的粗糙度为236.7 nm,在5 × 10-5 M维生素c的存在下,电抛光后钢试样的粗糙度降至140 nm。扫描电镜研究证实,低浓度和中等浓度的维生素C比高浓度的维生素C更能有效地提高水平和亮度。关键词:钢,电抛光,维生素C,扫描电镜,原子力显微镜,反射率。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A study of the morphology and optical properties of electro polished steel in the presence of Vitamin-C
The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations.   Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信