{"title":"维生素c对电抛光钢形貌和光学性能的影响","authors":"F. Abouzeid","doi":"10.5897/AJPAC2015.0631","DOIUrl":null,"url":null,"abstract":"The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations. \n \n \n \n Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.","PeriodicalId":7556,"journal":{"name":"African Journal of Pure and Applied Chemistry","volume":"67 1","pages":"135-145"},"PeriodicalIF":0.0000,"publicationDate":"2015-06-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A study of the morphology and optical properties of electro polished steel in the presence of Vitamin-C\",\"authors\":\"F. Abouzeid\",\"doi\":\"10.5897/AJPAC2015.0631\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations. \\n \\n \\n \\n Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.\",\"PeriodicalId\":7556,\"journal\":{\"name\":\"African Journal of Pure and Applied Chemistry\",\"volume\":\"67 1\",\"pages\":\"135-145\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2015-06-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"African Journal of Pure and Applied Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5897/AJPAC2015.0631\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"African Journal of Pure and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5897/AJPAC2015.0631","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
A study of the morphology and optical properties of electro polished steel in the presence of Vitamin-C
The studies of steel electrochemical polishing Electropolishing (EP) in orthophoshoric acid were performed by potentiodynamic polarization. Electropolishing was conducted in solution containing Vitamin C. Addition of Vitamin C to electropolishing solution results in a lower limiting current. Vitamin C concentration influence on electropolishing process and surface texture (AFM, SEM) and UV-VIS-NIR Spectroscopy was established. The results show that by increasing Vitamin C concentration from 2 × 10-5 to 5 × 10-5 M, roughness and reflectance of steel specimens decrease/increase respectively. The opposite trend is seen when the concentration increases to 10 × 10-5 M. The roughness of steel specimen before electropolishing is 236.7 nm and it will decrease to 140 nm by electropolishing in the presence of 5 × 10-5 M Vitamin C. A similar trend is also seen in reflection. The SEM study confirms that low and moderate concentration of Vitamin C was effective to enhance levelling and brightness more than higher concentrations.
Key words: Steel, electropolishing, Vitamin C, scanning electron microscope (SEM), atomic force microscope (AFM), reflectance.