研究了紫外光对用TiO2-K2O/天然沸石复合材料从核桃油制备生物柴油收率和特性的影响

M. T. Adiwibowo, I. Kustiningsih, A. B. Pitaloka, Wardalia Wardalia, Tati Jumiarti, Hani Mulyani
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引用次数: 0

摘要

本研究考察了紫外线照射对使用tio2 - k2o /天然沸石复合材料从核桃油中提取生物柴油的收率和物理特性的影响。用KOH活化天然沸石,并用tio2浸渍。用x射线衍射仪对形成的复合材料进行分析。以蜡烛油与甲醇的摩尔比为1:4、1:6、1:8,催化剂负载(w/w油)为2、4、6%,合成了生物柴油。XRD分析显示了锐钛矿、金红石、tio2、k2o和沸石的峰型。紫外光可提高生物柴油收率,在油甲醇摩尔比为1:8、催化剂负载为2%的条件下,生物柴油收率最高,为82.08%。生物柴油的物理性能符合国家标准SNI 7182:2015。GCMS结果表明,生物柴油中脂肪酸甲酯的主要成分为油酸甲酯、棕榈酸甲酯和亚油酸甲酯。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
THE EFFECT OF UV LIGHT ON THE YIELD AND CHARACTERISTICS OF BIODIESEL FROM CANDLENUT OIL USING A TiO2-K2O/NATURAL ZEOLITE COMPOSITE
This study examines the effect of UV irradiation on the yield and physical characteristics of biodiesel from candlenut oil using a TiO 2 -K 2 O/natural zeolite composite. Natural zeolite was activated with KOH and impregnated with TiO 2 . The formed composite was analyzed with an X-ray diffractometer. Biodiesel was synthesized with candlenut oil to methanol molar ratio and catalyst loading (w/w oil) 1:4, 1:6, 1:8, and 2, 4, and 6%, respectively. The XRD analysis shows peak patterns of anatase and rutile TiO 2 , K 2 O, and zeolite. UV light can increase biodiesel yield, with the highest yield at 82.08% at oil to methanol molar ratio of 1:8 and a catalyst loading of 2%. The physical properties of biodiesel are in accordance with national standard SNI 7182:2015. GCMS results shows that the main components of fatty acid methyl ester from biodiesel are methyl oleate, methyl palmitate, and methyl linoleate.
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