E. Antonelli, M. Andreeta, E. Botero, A. Hernandes
{"title":"厚膜激光烧结:两步工艺的证据","authors":"E. Antonelli, M. Andreeta, E. Botero, A. Hernandes","doi":"10.2174/1874846501306010001","DOIUrl":null,"url":null,"abstract":"The results for the sintering of Bi4Ti3O12 (BIT)-doped BaTi0.85Zr0.15O3 (BTZ) thick films, deposited by electro- phoresis, using as heating source a CO2 laser are presented. The thermal process associated to the laser scanning sintering (LSS) acted in a similar way as a two-step-sintering process. This characteristic together with the high heating rate al- lowed us to obtain thick films with an average grain size of 200 nm, high relative density (~96%) and with a homogene- ous microstructure. The X ray diffraction profile analysis show evidences for Bi 3+ replacing Ba 2+ at the A sites.","PeriodicalId":23072,"journal":{"name":"The Open Crystallography Journal","volume":"1 1","pages":"1-6"},"PeriodicalIF":0.0000,"publicationDate":"2013-09-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Thick Film Laser Sintering: An Evidence for Two-step Process\",\"authors\":\"E. Antonelli, M. Andreeta, E. Botero, A. Hernandes\",\"doi\":\"10.2174/1874846501306010001\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The results for the sintering of Bi4Ti3O12 (BIT)-doped BaTi0.85Zr0.15O3 (BTZ) thick films, deposited by electro- phoresis, using as heating source a CO2 laser are presented. The thermal process associated to the laser scanning sintering (LSS) acted in a similar way as a two-step-sintering process. This characteristic together with the high heating rate al- lowed us to obtain thick films with an average grain size of 200 nm, high relative density (~96%) and with a homogene- ous microstructure. The X ray diffraction profile analysis show evidences for Bi 3+ replacing Ba 2+ at the A sites.\",\"PeriodicalId\":23072,\"journal\":{\"name\":\"The Open Crystallography Journal\",\"volume\":\"1 1\",\"pages\":\"1-6\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2013-09-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"The Open Crystallography Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2174/1874846501306010001\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"The Open Crystallography Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2174/1874846501306010001","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Thick Film Laser Sintering: An Evidence for Two-step Process
The results for the sintering of Bi4Ti3O12 (BIT)-doped BaTi0.85Zr0.15O3 (BTZ) thick films, deposited by electro- phoresis, using as heating source a CO2 laser are presented. The thermal process associated to the laser scanning sintering (LSS) acted in a similar way as a two-step-sintering process. This characteristic together with the high heating rate al- lowed us to obtain thick films with an average grain size of 200 nm, high relative density (~96%) and with a homogene- ous microstructure. The X ray diffraction profile analysis show evidences for Bi 3+ replacing Ba 2+ at the A sites.