碳纳米结构离子源的微型质谱仪

J. Hwang, S.W. Park, J.B. Cho, K. Oh, S.S. Yang, Soonil Lee, K. Koh, K. Jung
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引用次数: 11

摘要

本文报道了采用碳纳米结构离子生成新方法的微飞行时间质谱仪的制备与实验。该装置由离子源和离子分离器组成。离子源通过场发射法产生电子。碳纳米结构具有良好的场发射性能。发射的电子与样品分子碰撞并使样品分子电离。这些离子被分离器加速。当离子按质量大小的顺序到达离子探测器时,产生电流输出信号。组装的微型TOF质谱仪尺寸为11 × 11 × 1mm3。实验是在真空室中进行的。将样品气体引入腔室,并在分离电极上施加适当的电压以实现离子加速。然后观察离子探测器发出的电流信号。实验结果验证了所制备的微型质谱仪中离子源和离子分离器的可行性
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The Micro Mass Spectrometer with A Carbon Nano Structure Ion Source
This paper reports the fabrication and experiment of a micro time of flight (TOF) mass spectrometer adopting a new ion generation method using a carbon nanostructure. The device is composed of an ion source and an ion separator. The ion source generates electrons by the field emission method. Carbon nanostructure has good field emission property. The emitted electrons collide with sample molecules and ionize the sample molecules. These ions are accelerated by separator. The current output signal is generated when the ions reach the ion detector in the order of mass size. The size of the assembled micro TOF mass spectrometer is 11 times 11 times 1 mm3. The experiment is performed in a vacuum chamber. The sample gas is introduced to the chamber and suitable voltages are applied to separation electrodes for the ion acceleration. Then we observe the current signal from the ion detector. The experimental result verifies the feasibility of the ion source and the ion separator included in the fabricated micro mass spectrometer
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