气相色谱-质谱法分析水馏索内奇精油

Mwaura J. Njuguna
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引用次数: 1

摘要

从肯尼亚穆兰加县坎达拉副县的植物样本中采集了索内奇奥·马尼的叶子。收集叶的目的是提取和分析马尾草的精油。这些叶子被运送到肯尼亚山大学的生药学实验室。用自来水冲洗叶子,用蒸馏水冲洗以去除物理和化学污染物。它们在实验室的工作台上风干7天,以失去90%的水分含量。从200.000 g干叶中提取精油(Eos),用Clavenger装置加氢蒸馏8小时。经计算,其精油提取率为0.01%。采用气相色谱-质谱联用仪对精油成分进行定性和定量分析。总离子图谱中发现的化合物有:3-蒈烯(40%)、柠檬烯(35.48%)、1-十一醇(8.0%)、β-蒎烯(6.4%)、薄荷醇(1.6%)、β-花仙花烯(1.1%)、长叶烯(0.78%)和α-萜烯(0.5%)。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Gas Chromatography-Mass Spectrometry Analysis of Hydrodistilled Essentials Oils from Solanecio manii
The leaves of Solanecio manii were collected from sampled plants in Kandara Sub-County Muranga County in Kenya. The aim of collection of the leaves was to carry out the extraction and analysis of essential oils from S. manii. The leaves were transported to the pharmacognosy laboratory at the Mount Kenya University. The leaves were washed with running tap water and rinsed with distilled water to remove physical and chemical contaminants. They were air dried on the laboratory benches for seven days to lose 90% of moisture content. The essential oils (Eos) were extracted from 200.000 g of dry leaves by hydrodistillation using the Clavenger apparatus for 8 hours. The rate of essential oil production from the leaves was computed and found to be 0.01%. GC-MS instrument was utilized to analyse the qualitative and quantitative composition of essential oils. The compounds that were found present in the total ion chromatogram were, 3-Carene (40%), Limonene (35.48%), 1-undecanol (8.0%), β-pinene (6.4%), Menthol (1.6%), β-Cymene (1.1%) Longifolene (0.78%) and α-terpenolene (0.5%).
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