{"title":"四氯酸四乙基铵(II)的晶体结构和分子结构","authors":"G. Stucky, J. Folkers, T. Kistenmacher","doi":"10.1107/S0365110X67004268","DOIUrl":null,"url":null,"abstract":"The crystal structure of tetraethylammonium tetrachloronickelate(II) has been determined by fullmatrix least-squares refinement of three-dimensional Mo Kct intensity data. The space group is P42/nmc, with Z=2. Cell constants are a=b= 9.05, c= 15\"01 A. The corresponding cobalt salt is isomorphous, with a=b=9.00, c= 14.97/~. The tetraethylammonium groups were found to be disordered about intersecting mirror planes. Qualitatively, the distortions of the anion from tetrahedral symmetry are similar to those of the CoC1 lanion in Cs3CoC15.","PeriodicalId":7001,"journal":{"name":"Acta Crystallographica","volume":"64 1","pages":"1064-1070"},"PeriodicalIF":0.0000,"publicationDate":"1967-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"83","resultStr":"{\"title\":\"The crystal and molecular structure of tetraethylammonium tetrachloronickelate(II)\",\"authors\":\"G. Stucky, J. Folkers, T. Kistenmacher\",\"doi\":\"10.1107/S0365110X67004268\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The crystal structure of tetraethylammonium tetrachloronickelate(II) has been determined by fullmatrix least-squares refinement of three-dimensional Mo Kct intensity data. The space group is P42/nmc, with Z=2. Cell constants are a=b= 9.05, c= 15\\\"01 A. The corresponding cobalt salt is isomorphous, with a=b=9.00, c= 14.97/~. The tetraethylammonium groups were found to be disordered about intersecting mirror planes. Qualitatively, the distortions of the anion from tetrahedral symmetry are similar to those of the CoC1 lanion in Cs3CoC15.\",\"PeriodicalId\":7001,\"journal\":{\"name\":\"Acta Crystallographica\",\"volume\":\"64 1\",\"pages\":\"1064-1070\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1967-12-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"83\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Crystallographica\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1107/S0365110X67004268\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Crystallographica","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1107/S0365110X67004268","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
The crystal and molecular structure of tetraethylammonium tetrachloronickelate(II)
The crystal structure of tetraethylammonium tetrachloronickelate(II) has been determined by fullmatrix least-squares refinement of three-dimensional Mo Kct intensity data. The space group is P42/nmc, with Z=2. Cell constants are a=b= 9.05, c= 15"01 A. The corresponding cobalt salt is isomorphous, with a=b=9.00, c= 14.97/~. The tetraethylammonium groups were found to be disordered about intersecting mirror planes. Qualitatively, the distortions of the anion from tetrahedral symmetry are similar to those of the CoC1 lanion in Cs3CoC15.
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