{"title":"全氟-2,5-二甲基-3,6-二氧杂烷酸三乙氧基硅基丙酰胺(Fluorosam-39)和氟橡胶SKF-32的合成及其热特性","authors":"S. Krukovsky","doi":"10.17677/FN20714807.2019.02.02","DOIUrl":null,"url":null,"abstract":"A new methodology for obtainment of compositions based on Fluorosam-39 monomer (triethoxysilylpropylamide perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid) with fluororubber SKF-32 (vinylidene fluoride with trifluorochloroethylene co-polymer) in the presence of AMEO (γaminopropyltriethoxysilane) as a catalyst and co-reactant was developed. Content of fluororubber in compositions varied from 10 to 55% (mass.). Thermal properties of the composition, obtained from Fluorosam-39:SKF-32:AMEO at the ratio 45,5: 48,5: 6 (mass.%) were measured using thermomechanical and thermogravimetric analysis methods.","PeriodicalId":12217,"journal":{"name":"Fluorine Notes","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2019-04-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Obtainment and thermal characteristics of the composition of perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid triethoxysilylpropylamide (Fluorosam-39) and fluororubber SKF-32\",\"authors\":\"S. Krukovsky\",\"doi\":\"10.17677/FN20714807.2019.02.02\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A new methodology for obtainment of compositions based on Fluorosam-39 monomer (triethoxysilylpropylamide perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid) with fluororubber SKF-32 (vinylidene fluoride with trifluorochloroethylene co-polymer) in the presence of AMEO (γaminopropyltriethoxysilane) as a catalyst and co-reactant was developed. Content of fluororubber in compositions varied from 10 to 55% (mass.). Thermal properties of the composition, obtained from Fluorosam-39:SKF-32:AMEO at the ratio 45,5: 48,5: 6 (mass.%) were measured using thermomechanical and thermogravimetric analysis methods.\",\"PeriodicalId\":12217,\"journal\":{\"name\":\"Fluorine Notes\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-04-14\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Fluorine Notes\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.17677/FN20714807.2019.02.02\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Fluorine Notes","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17677/FN20714807.2019.02.02","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Obtainment and thermal characteristics of the composition of perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid triethoxysilylpropylamide (Fluorosam-39) and fluororubber SKF-32
A new methodology for obtainment of compositions based on Fluorosam-39 monomer (triethoxysilylpropylamide perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid) with fluororubber SKF-32 (vinylidene fluoride with trifluorochloroethylene co-polymer) in the presence of AMEO (γaminopropyltriethoxysilane) as a catalyst and co-reactant was developed. Content of fluororubber in compositions varied from 10 to 55% (mass.). Thermal properties of the composition, obtained from Fluorosam-39:SKF-32:AMEO at the ratio 45,5: 48,5: 6 (mass.%) were measured using thermomechanical and thermogravimetric analysis methods.
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