用不同峰谱分析测定ZnO纳米颗粒的晶形参数

M. S. H. Choudhury, Mohammad Shahidul Alam, Md Mizanul Islam, T. Soga, M. Shafiul Alam, M. Rafiqul Islam
{"title":"用不同峰谱分析测定ZnO纳米颗粒的晶形参数","authors":"M. S. H. Choudhury, Mohammad Shahidul Alam, Md Mizanul Islam, T. Soga, M. Shafiul Alam, M. Rafiqul Islam","doi":"10.1109/ICISET.2018.8745655","DOIUrl":null,"url":null,"abstract":"In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ε) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.","PeriodicalId":6608,"journal":{"name":"2018 International Conference on Innovations in Science, Engineering and Technology (ICISET)","volume":"4 1","pages":"257-261"},"PeriodicalIF":0.0000,"publicationDate":"2018-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis\",\"authors\":\"M. S. H. Choudhury, Mohammad Shahidul Alam, Md Mizanul Islam, T. Soga, M. Shafiul Alam, M. Rafiqul Islam\",\"doi\":\"10.1109/ICISET.2018.8745655\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ε) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.\",\"PeriodicalId\":6608,\"journal\":{\"name\":\"2018 International Conference on Innovations in Science, Engineering and Technology (ICISET)\",\"volume\":\"4 1\",\"pages\":\"257-261\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-10-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2018 International Conference on Innovations in Science, Engineering and Technology (ICISET)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ICISET.2018.8745655\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2018 International Conference on Innovations in Science, Engineering and Technology (ICISET)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICISET.2018.8745655","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 2

摘要

在本研究中,采用叶片涂层技术获得ZnO薄膜,并用x射线衍射(XRD)分析对其进行表征。分析表明,ZnO颗粒为结晶性质,具有六方纤锌矿结构。利用x射线峰谱分析(XPPA)对晶体发育进行了验证。采用Williamson-Hall (W-H)和尺寸-应变图(SSP)分析了ZnO纳米颗粒的晶粒尺寸(D)和晶格应变(ε)。进一步研究了XRD峰,确定了一些物理参数,包括晶格应变、晶体应力和能量密度。本文采用几种W-H模型的修正形式对上述参数进行了计算,并对各种方法得到的参数结果进行了比较。研究表明,各种模型计算出的晶体参数基本相似。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis
In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ε) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信