用operando衍射和射线照相技术研究了氦气作为工艺气体对Ti-6Al-4V激光粉末床熔合的影响

C. Pauzon, S. Van Petegem, E. Hryha, Cynthia Sin Ting Chang, S. Hocine, H. Van Swygenhoven, C. de Formanoir, S. Dubiez-Le Goff
{"title":"用operando衍射和射线照相技术研究了氦气作为工艺气体对Ti-6Al-4V激光粉末床熔合的影响","authors":"C. Pauzon, S. Van Petegem, E. Hryha, Cynthia Sin Ting Chang, S. Hocine, H. Van Swygenhoven, C. de Formanoir, S. Dubiez-Le Goff","doi":"10.1080/26889277.2022.2081622","DOIUrl":null,"url":null,"abstract":"Abstract The utilisation of helium as process gas in laser powder bed fusion limits the generation of Ti-6Al-4V hot and incandescent spatters and enhances their cooling rate. In the present study, operando X-ray diffraction using synchrotron X-rays permits to verify that the cooling rates experienced by the deposited material are not significantly affected by the process gas unlike spatters. Topography measurements of the top printed surface reveal lower roughness of He-produced samples, attributed to the previously observed reduction of spatters with He and thus a reduction of redepositions on the powder bed and printed surfaces. Operando radiography provides with insights on the spatter formation mechanisms namely particle entrainment, agglomeration, melting and spheroidization. Highlights The top surface average roughness of samples produced with He is lower than that of Ar equivalent Deposited Ti-6Al-4V cooling rates during LPBF are not significantly affected by the use of He Grain size and orientation of Ti-6Al-4V is similar when processing under Ar, He, and a mixture of both Operando radiography permits to identify the mechanisms of Ti-6Al-4V spatter formation","PeriodicalId":32608,"journal":{"name":"European Journal of Materials Science and Engineering","volume":"7 1","pages":"422 - 435"},"PeriodicalIF":0.0000,"publicationDate":"2022-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Effect of helium as process gas on laser powder bed fusion of Ti-6Al-4V studied with operando diffraction and radiography\",\"authors\":\"C. Pauzon, S. Van Petegem, E. Hryha, Cynthia Sin Ting Chang, S. Hocine, H. Van Swygenhoven, C. de Formanoir, S. Dubiez-Le Goff\",\"doi\":\"10.1080/26889277.2022.2081622\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract The utilisation of helium as process gas in laser powder bed fusion limits the generation of Ti-6Al-4V hot and incandescent spatters and enhances their cooling rate. In the present study, operando X-ray diffraction using synchrotron X-rays permits to verify that the cooling rates experienced by the deposited material are not significantly affected by the process gas unlike spatters. Topography measurements of the top printed surface reveal lower roughness of He-produced samples, attributed to the previously observed reduction of spatters with He and thus a reduction of redepositions on the powder bed and printed surfaces. Operando radiography provides with insights on the spatter formation mechanisms namely particle entrainment, agglomeration, melting and spheroidization. Highlights The top surface average roughness of samples produced with He is lower than that of Ar equivalent Deposited Ti-6Al-4V cooling rates during LPBF are not significantly affected by the use of He Grain size and orientation of Ti-6Al-4V is similar when processing under Ar, He, and a mixture of both Operando radiography permits to identify the mechanisms of Ti-6Al-4V spatter formation\",\"PeriodicalId\":32608,\"journal\":{\"name\":\"European Journal of Materials Science and Engineering\",\"volume\":\"7 1\",\"pages\":\"422 - 435\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-12-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"European Journal of Materials Science and Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/26889277.2022.2081622\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"European Journal of Materials Science and Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/26889277.2022.2081622","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

摘要

在激光粉末床熔合过程中,氦气的使用限制了Ti-6Al-4V热溅射和白炽溅射的产生,提高了其冷却速度。在本研究中,使用同步加速器x射线的operando x射线衍射允许验证沉积材料所经历的冷却速率不像飞溅那样受到工艺气体的显着影响。顶部印刷表面的形貌测量显示,He生产样品的粗糙度较低,这归因于先前观察到的He减少了飞溅,从而减少了粉末床和印刷表面的重新定位。Operando射线摄影提供了对飞溅形成机制的见解,即颗粒夹带,团聚,熔化和球化。He制备的样品的表面平均粗糙度低于Ar,在LPBF过程中沉积Ti-6Al-4V的冷却速度没有受到He的显著影响,当在Ar、He和两者的混合下加工时,Ti-6Al-4V的晶粒尺寸和取向相似,Operando射线照相允许识别Ti-6Al-4V飞溅形成的机制
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of helium as process gas on laser powder bed fusion of Ti-6Al-4V studied with operando diffraction and radiography
Abstract The utilisation of helium as process gas in laser powder bed fusion limits the generation of Ti-6Al-4V hot and incandescent spatters and enhances their cooling rate. In the present study, operando X-ray diffraction using synchrotron X-rays permits to verify that the cooling rates experienced by the deposited material are not significantly affected by the process gas unlike spatters. Topography measurements of the top printed surface reveal lower roughness of He-produced samples, attributed to the previously observed reduction of spatters with He and thus a reduction of redepositions on the powder bed and printed surfaces. Operando radiography provides with insights on the spatter formation mechanisms namely particle entrainment, agglomeration, melting and spheroidization. Highlights The top surface average roughness of samples produced with He is lower than that of Ar equivalent Deposited Ti-6Al-4V cooling rates during LPBF are not significantly affected by the use of He Grain size and orientation of Ti-6Al-4V is similar when processing under Ar, He, and a mixture of both Operando radiography permits to identify the mechanisms of Ti-6Al-4V spatter formation
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
21
审稿时长
10 weeks
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信