海藻酸盐-壳聚糖膜作为pH指示剂的固定化海芋叶提取物的表征

N. Ismillayli, Septia Hadiyati, Rahayu Juniharti, D. Hermanto
{"title":"海藻酸盐-壳聚糖膜作为pH指示剂的固定化海芋叶提取物的表征","authors":"N. Ismillayli, Septia Hadiyati, Rahayu Juniharti, D. Hermanto","doi":"10.1063/5.0059608","DOIUrl":null,"url":null,"abstract":"An easy, simple and eco-friendly pH indicator from immobilized Rhoeo discolor leaf extract on alginate-chitosan membrane was developed. Rhoeo discolor leaf extract in ethanol was immobilized in the alginate-chitosan membrane by entrapment technique. The membrane was prepared at a pH of 5.2 with a mass ratio of alginate and chitosan of 1:1. Then, the immobilized extract in the membrane was tested in a pH solution of 2 to 8. The resulting pH indicator was characterized by UV-Vis and FTIR spectroscopy. Furthermore, biodegradability tests in soil medium was carried out. The color change was observed at pH 2 to 8. FTIR spectra showed that interaction of alginate and chitosan in membrane was occurred through electrostatic interaction between carboxylate group and protonated amine, while the immobilized membraned showed no additional functional groups that indicated there is no chemical interaction between leaf extract and alginate-chitosan membrane. The leaf extract was trapped in a three-dimensional network of alginate-chitosan membrane. Biodegradability test on soil medium for 21 days showed a membrane degradation of 23.07%. Therefore, the obtained pH indicator is suitable for eco-friendly pH testing tool.","PeriodicalId":13712,"journal":{"name":"INTERNATIONAL CONFERENCE ON ENERGY AND ENVIRONMENT (ICEE 2021)","volume":"26 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-09-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Characterization of immobilized Rhoeo discolor (L’Hér.) hance leaf extract in alginate-chitosan membrane as a pH indicator\",\"authors\":\"N. Ismillayli, Septia Hadiyati, Rahayu Juniharti, D. Hermanto\",\"doi\":\"10.1063/5.0059608\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"An easy, simple and eco-friendly pH indicator from immobilized Rhoeo discolor leaf extract on alginate-chitosan membrane was developed. Rhoeo discolor leaf extract in ethanol was immobilized in the alginate-chitosan membrane by entrapment technique. The membrane was prepared at a pH of 5.2 with a mass ratio of alginate and chitosan of 1:1. Then, the immobilized extract in the membrane was tested in a pH solution of 2 to 8. The resulting pH indicator was characterized by UV-Vis and FTIR spectroscopy. Furthermore, biodegradability tests in soil medium was carried out. The color change was observed at pH 2 to 8. FTIR spectra showed that interaction of alginate and chitosan in membrane was occurred through electrostatic interaction between carboxylate group and protonated amine, while the immobilized membraned showed no additional functional groups that indicated there is no chemical interaction between leaf extract and alginate-chitosan membrane. The leaf extract was trapped in a three-dimensional network of alginate-chitosan membrane. Biodegradability test on soil medium for 21 days showed a membrane degradation of 23.07%. Therefore, the obtained pH indicator is suitable for eco-friendly pH testing tool.\",\"PeriodicalId\":13712,\"journal\":{\"name\":\"INTERNATIONAL CONFERENCE ON ENERGY AND ENVIRONMENT (ICEE 2021)\",\"volume\":\"26 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-09-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"INTERNATIONAL CONFERENCE ON ENERGY AND ENVIRONMENT (ICEE 2021)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1063/5.0059608\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"INTERNATIONAL CONFERENCE ON ENERGY AND ENVIRONMENT (ICEE 2021)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/5.0059608","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

以海藻酸盐-壳聚糖膜固定化红草叶提取物为原料,研制了一种简便、环保的pH指示剂。采用包埋法将水芹脱色叶提取液固定在海藻酸-壳聚糖膜中。在pH为5.2,海藻酸盐与壳聚糖的质量比为1:1的条件下制备膜。然后,在pH为2 ~ 8的溶液中测试膜中固定的提取物。用紫外可见光谱和红外光谱对所得pH指示剂进行了表征。在土壤介质中进行了生物降解试验。在pH值2 ~ 8时观察颜色变化。傅里叶红外光谱显示,海藻酸盐与壳聚糖在膜内的相互作用是通过羧酸基与质子化胺的静电相互作用发生的,而固定化膜没有发现额外的官能团,表明叶片提取物与海藻酸盐-壳聚糖膜之间没有化学相互作用。叶片提取物被捕获在海藻酸盐-壳聚糖膜的三维网络中。在土壤培养基上进行21 d的生物降解试验,膜降解率为23.07%。因此,所得pH指示剂适用于环保型pH测试工具。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Characterization of immobilized Rhoeo discolor (L’Hér.) hance leaf extract in alginate-chitosan membrane as a pH indicator
An easy, simple and eco-friendly pH indicator from immobilized Rhoeo discolor leaf extract on alginate-chitosan membrane was developed. Rhoeo discolor leaf extract in ethanol was immobilized in the alginate-chitosan membrane by entrapment technique. The membrane was prepared at a pH of 5.2 with a mass ratio of alginate and chitosan of 1:1. Then, the immobilized extract in the membrane was tested in a pH solution of 2 to 8. The resulting pH indicator was characterized by UV-Vis and FTIR spectroscopy. Furthermore, biodegradability tests in soil medium was carried out. The color change was observed at pH 2 to 8. FTIR spectra showed that interaction of alginate and chitosan in membrane was occurred through electrostatic interaction between carboxylate group and protonated amine, while the immobilized membraned showed no additional functional groups that indicated there is no chemical interaction between leaf extract and alginate-chitosan membrane. The leaf extract was trapped in a three-dimensional network of alginate-chitosan membrane. Biodegradability test on soil medium for 21 days showed a membrane degradation of 23.07%. Therefore, the obtained pH indicator is suitable for eco-friendly pH testing tool.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信