辣木叶柄提取物纳米银的合成及表征

I. R, Muhammad Tasjiddin Teheni, W. Syafriah
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引用次数: 0

摘要

开发植物提取物作为合成纳米银的还原剂已成为研究人员关注的焦点。以辣木叶柄提取物为原料,采用生物还原法制备纳米银。通过紫外可见吸收光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)和x射线衍射(XRD)对AgNPs进行了表征。研究结果表明,AgNO3初始浓度和孵育时间的增加影响了AgNPs表面等离子体共振(SPR)趋势的吸收模式。官能团分析结果显示酮基(1741 cm-1)由羟基(3415 cm-1)衍生而来。用XRD对AgNPs的晶体结构进行了表征。基于Debye-Scherer方程的晶体测量估计为15.59 nm,估计为立方体晶体形式。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Silver Nanoparticles from the Leaf Stalk Extract of Moringa oleifera
The exploitation of plant extract as a reducing agent for synthetic silver nanoparticles has become the main focus of researchers. This study aimed to synthesize silver nanoparticles (AgNPs) from Moringa oleifera leaf stalk extract via bio-reduction. The AgNPs were characterized through ultraviolet-visible absorption spectroscopy (UV-Vis), Fourier transforms infrared spectroscopy (FTIR), and X-ray diffraction (XRD). The research results indicated that an increase in the initial AgNO3 concentration and incubation time had affected the absorption pattern of the surface plasmon resonance (SPR) trend of AgNPs. The results of the functional group analysis revealed the formation of the ketone group (1741 cm-1), which was derived from hydroxyl groups (3415 cm-1). The crystal structure of AgNPs was characterized using XRD. The estimation of the crystal measurement based on the Debye-Scherer equation was 15.59 nm, which was estimated as having a cube crystal form.
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