快速、 高精度可见光-近红外透射光谱测量技术研究

王圣浩, 刘世杰, 王微微, 张志刚
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引用次数: 0

摘要

本文在传统分光光度法框架的基础上,提出了一种快速、高精度测量可见光-近红外波段透射光谱的新技术,其主要特点是在测量过程中,光栅单色仪输出波长连续增加,同时光电探测器并行连续采集数据。初步实验结果表明,该方法可将透射光谱测量时间缩短至传统分光光度法的50%,相对误差为0.070%,重复性误差为0.042%。与目前常用的可见光-近红外透射光谱测量方法(分光光度法、基于多通道光谱仪的方法和傅立叶变换光谱仪的方法)相比,该方法具有以下优点:一是测量速度大大加快,可见-近红外透射光谱的快速测量具有广阔的应用前景,在动态环境中具有广泛的应用前景;其次,测量精度高(0.1%-0.3%),最后,由于光栅单色仪的电机在测量过程中连续旋转,测量系统具有很高的机械稳定性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
快速、 高精度可见光-近红外透射光谱测量技术研究
In this paper, based on the framework of traditional spectrophotometry, we put forward a novel fast and high-accuracy technique for measuring transmittance spectrum in VIS-NIR wave range, its key feature is that during the measurement procedure, the output wavelength of the grating monochromator is kept increasing continuously and at the same time, the photoelectric detectors execute a concurrently continuous data acquisition routine. Initial experiment result shows that the newly proposed technique could shorten the time consumed for measuring the transmittance spectrum down to 50% that of the conventional spectrophotometric method, a relative error of 0.070% and a repeatability error of 0.042% are generated. Compared with the current mostly used techniques (spectrophotometry, methods based on multi-channel spectrometer and strategy using Fourier transform spectrometer) for obtaining transmittance spectrum in VIS-NIR, the new strategy has at all once the following advantages, firstly the measuring speed could be greatly quicken, fast measurement of transmittance spectrum in VIS-NIR is therefore promising, which would find wide application in dynamic environment, secondly high measuring accuracy (0.1%-0.3%) is available, and finally the measuring system has high mechanical stability because the motor of the grating monochromator is rotating continuously during the measurement.
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