椰壳灰(CHA)增强聚酯复合材料物理力学性能及动态力学性能评价

T. Ipilakyaa
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引用次数: 0

摘要

利用研制的CHA增强聚合物复合材料进行了物理性能评价和动态力学分析(DMA)。对预处理后的CHA进行筛分分析,得到75µm、150µm和300µm的粒径。这些颗粒分别以5%、10%、15%、20%和25%的不同组分作为聚酯复合材料的增强剂。催化剂和促进剂分别为过氧化甲乙酮和环烷酸钴。粒径为150 μm的复合材料密度在0.9792 ~ 1.2561 g/cm3之间,低于粒径为75μm和300μm的复合材料。结果还表明,随着样品在蒸馏水中浸泡时间的延长,样品的吸水率均有所增加,在0 ~ 2000 E′/MPa以上范围内。然而,25%的增强对所有粒径都有更好的效果。贮藏模量、损耗模量和力学损耗因子随补强率、温度和频率的变化有明显的变化。增强率为15%的复合材料表现出较好的效果,可用于航空航天和汽车工业的内饰件材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Evaluation of physical and dynamic mechanical properties of coconut husk ash (CHA) reinforced polyester composites
The evaluation of physical and dynamic mechanical analysis (DMA) properties was carried out using developed CHA Reinforced Polymer Composite. Sieve analysis of pretreated CHA was done to obtain 75 µm, 150 µm and 300 µm particles sizes. These particles were used at varying compositions of 5%, 10%, 15%, 20% and 25% as reinforcements for polyester composites. The catalyst and accelerator used were Methyl Ethyl Ketone Peroxide and Cobalt Naphthenate respectively. The densities of the evaluated composites made with 150 μm particles were found to be less dense with values ranging from 0.9792 g/cm3 to 1.2561 g/cm3 than those made with 75μm and 300μm. The results also show that the percentage water absorbed by samples increased, ranging from 0 to over 2000 E’/MPa for all percentage reinforcements of CHA, with an increase in the duration of immersion of the samples in distilled water. However, 25% reinforcement had better results for all particle sizes. There were obvious variations of storage modulus, loss modulus and mechanical loss factor with percentage weight of reinforcement, temperature and frequency. The composite with 15 % reinforcement displayed better results and can be used as a material for interior components in aerospace and automobile industries.
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