P. Shahgaldian , P. Goreloff , R. Lamartine , A.W. Coleman
{"title":"异丙基杯[6]芳烃薄膜结晶过程随时间变化的SPM研究","authors":"P. Shahgaldian , P. Goreloff , R. Lamartine , A.W. Coleman","doi":"10.1016/S1463-0184(02)00004-7","DOIUrl":null,"url":null,"abstract":"<div><p>The crystallization process during annealing at 100°C of thin films of <em>iso</em>-propyl-calix-[6]-arene has been studied using topographic and lateral force imaging of contact mode scanning probe microscopy. The crystallization proceeds from sub-micron crystallites with mass migration to form large crystalline wall-like structures several microns in width and over 100 μm in length. During the annealing these wall-like structures compact with a concomitant decrease in width. Lateral force imaging shows the presence of moiré-pattern like zones of high and low friction forces.</p></div>","PeriodicalId":10766,"journal":{"name":"Crystal Engineering","volume":"5 1","pages":"Pages 47-58"},"PeriodicalIF":0.0000,"publicationDate":"2002-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S1463-0184(02)00004-7","citationCount":"1","resultStr":"{\"title\":\"An SPM study of time dependent crystallization processes in iso-propyl-calix-[6]-arene thin films\",\"authors\":\"P. Shahgaldian , P. Goreloff , R. Lamartine , A.W. Coleman\",\"doi\":\"10.1016/S1463-0184(02)00004-7\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>The crystallization process during annealing at 100°C of thin films of <em>iso</em>-propyl-calix-[6]-arene has been studied using topographic and lateral force imaging of contact mode scanning probe microscopy. The crystallization proceeds from sub-micron crystallites with mass migration to form large crystalline wall-like structures several microns in width and over 100 μm in length. During the annealing these wall-like structures compact with a concomitant decrease in width. Lateral force imaging shows the presence of moiré-pattern like zones of high and low friction forces.</p></div>\",\"PeriodicalId\":10766,\"journal\":{\"name\":\"Crystal Engineering\",\"volume\":\"5 1\",\"pages\":\"Pages 47-58\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2002-03-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/S1463-0184(02)00004-7\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Crystal Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1463018402000047\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Crystal Engineering","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1463018402000047","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
An SPM study of time dependent crystallization processes in iso-propyl-calix-[6]-arene thin films
The crystallization process during annealing at 100°C of thin films of iso-propyl-calix-[6]-arene has been studied using topographic and lateral force imaging of contact mode scanning probe microscopy. The crystallization proceeds from sub-micron crystallites with mass migration to form large crystalline wall-like structures several microns in width and over 100 μm in length. During the annealing these wall-like structures compact with a concomitant decrease in width. Lateral force imaging shows the presence of moiré-pattern like zones of high and low friction forces.
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